Lead ion responsive smart membrane and preparation method thereof, and method for detecting lead ions in water samples
A smart membrane and lead ion technology, which is applied in the field of lead ion detection, can solve the problems of complicated membrane structure, difficulty in control, and cumbersome preparation process, and achieve the effects of improving lead ion response ability, appropriate membrane pore size, and simple preparation process
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Embodiment 1
[0050] In this example, a series of poly(N-isopropylacrylamide-co-benzo-18-crown-6 acrylamide) (P(NIPAM-co-B18C6Am)) (PNB) nano The microspheres are sequentially recorded as 1#~4#PNB nano-microspheres.
[0051] (1) Preparation of 1#PNB nanospheres
[0052] Using N-isopropylacrylamide and benzo-18-crown-6 acrylamide as raw materials, N,N-methylenebisacrylamide as crosslinking agent, and 2,2-azobisisobutylamidine di Hydrochloride is the initiator. Add the raw materials, cross-linking agent, initiator and deionized water into the single-necked flask, stir evenly to form a mixed solution, and then pass high-purity nitrogen into the single-necked flask for 60 minutes to remove the oxygen in the single-necked flask. Seal the single-necked flask, place it in a constant temperature water bath at 70°C and stir for 4 hours, filter the resulting reaction solution, and centrifuge the filtrate at a speed of 12000r / min. After the centrifugation is completed, remove the supernatant and add ...
Embodiment 2
[0076] In this example, the preparation method of the lead ion-responsive smart membrane is basically the same as that of Comparative Example 2, except that the mass ratio of 1#PNB nano-microsphere dry powder to polyethersulfone powder is 15:100, and the obtained The lead ion-responsive smart membrane is denoted as M-3.
Embodiment 3
[0078] In this example, the preparation method of the lead ion-responsive smart film is basically the same as that of Comparative Example 2, the difference is only that: 1#PNB nano-microsphere dry powder is replaced by 2#PNB nano-microsphere dry powder, and 2#PNB nano-microsphere dry powder is replaced by 2#PNB nano-microsphere dry powder. The mass ratio of spherical dry powder to polyethersulfone powder is 15:100, and the prepared lead ion-responsive smart membrane is designated as M-4.
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