A kind of composite surfactant containing quaternary ammonium salt and application thereof
A surfactant and quaternary ammonium salt technology, applied in the field of surfactant preparation, can solve the problems of harsh conditions, flocculation and stratification, and easy precipitation, so as to simplify the production process and improve production efficiency
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Embodiment 1
[0024] The preparation of embodiment 1 composite surfactant containing quaternary ammonium salt
[0025] The weight ratio of quaternary ammonium salt surfactant and oleaginous resin oil surfactant is 1:1 mixes and promptly obtains described composite surfactant containing quaternary ammonium salt; Described quaternary ammonium salt surfactant is Cetyltrimethylammonium chloride;
[0026] Described oleaginous resin oil surfactant is prepared by following method:
[0027] (1) Mix oleoresin oil and fumaric acid in a reaction kettle at a weight ratio of 1:0.3, and then adjust the temperature to 200°C for 4 hours to obtain fumaric acid modified oleoresin oil.
[0028] (2) Mix fumaric acid modified oleoresin oil, deionized water and xylitol in a weight ratio of 1:1.5:0.5 in the reaction kettle, and the added weight is 3% of the weight of fumaric acid modified oleoresin oil Zinc sulfate catalyst, and then adjust the temperature to 240 ° C for 4 hours, after cooling, the oleaginous r...
Embodiment 2
[0029] The preparation of embodiment 2 composite surfactant containing quaternary ammonium salt
[0030] The weight ratio of quaternary ammonium salt surfactant and oleaginous resin oil surfactant is 2:1 and mixes and obtains described composite surfactant containing quaternary ammonium salt; Described quaternary ammonium salt surfactant is Cetyltrimethylammonium chloride;
[0031] Described oleaginous resin oil surfactant is prepared by following method:
[0032] (1) Mix olean resin oil and fumaric acid in a reaction kettle at a weight ratio of 1:0.5, and then adjust the temperature to 180°C for 5 hours to obtain fumaric acid modified oleoresin oil.
[0033] (2) In the reactor, mix fumaric acid modified oleoresin oil, deionized water and xylitol in a weight ratio of 1:1:0.6, and the added weight is 5% of the weight of fumaric acid modified oleoresin oil The catalyst zinc sulfate, and then adjust the temperature to 220 ° C for 3 hours, after cooling, the oleaginous resin oil...
Embodiment 3
[0034] The preparation of embodiment 3 composite surfactant containing quaternary ammonium salt
[0035] The weight ratio of quaternary ammonium salt surfactant and oleaginous resin oil surfactant is 1:2 mixes to obtain described composite surfactant containing quaternary ammonium salt; Described quaternary ammonium salt surfactant is Cetyltrimethylammonium chloride;
[0036] Described oleaginous resin oil surfactant is prepared by following method:
[0037] (1) Mix oleoresin oil and fumaric acid in a reaction kettle at a weight ratio of 1:0.2, and then adjust the temperature to 220°C for 3 hours to obtain fumaric acid modified oleoresin oil.
[0038] (2) In the reactor, mix fumaric acid modified oleoresin oil, deionized water and xylitol in a weight ratio of 1:1:0.3, and the added weight is 2% of the weight of fumaric acid modified oleoresin oil The catalyst zinc sulfate, and then adjust the temperature to 250 ° C for 5 hours, after cooling, the oleaginous resin oil surfact...
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