An ideal two-dimensional Fermi liquid system bi 2 o 2 Se single crystal and its preparation method and application
A single crystal and reaction technology, applied in the directions of single crystal growth, single crystal growth, chemical instruments and methods, etc., can solve the problem of a small number of crystal materials, and achieve the effects of low cost, excellent crystal quality, and simple preparation method.
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[0062]Example 2. Using Bi2O3, Bi, Se are raw materials to grow Bi by solidification and crystallization method2O2Se crystal
[0063]Weigh 0.01mol Bi2O3The powder (4.6608g), 0.01mol Bi powder (2.0900g), 0.015 mol Se powder (1.1845g), mix evenly and put them into a prepared quartz tube (length 10cm, diameter 2cm), using a mechanical pump, The molecular pump is evacuated and sealed, and then the sealed quartz tube is fixed on the pull rod of the molten salt pulling furnace. The reaction temperature of the raw materials is set to 550℃, and the reaction time is 48h, and then the temperature is raised to 950℃, at 950℃ Keep holding for 24h to melt uniformly, then cool down at a rate of 2℃ / h, after a 10-day growth cycle, naturally cool down to obtain Bi2O2Se block, dissociate to obtain millimeter-level Bi with high quality2O2Se single crystal, the maximum size is about 2mm, such asfigure 2(a) Shown.
[0064]Such asfigure 2As shown in (b), the X-ray diffraction test (XRD) analysis shows that the c...
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