226 results about "Crystalline materials" patented technology

Crystal growth systems with a baffle are provided. In one example, a crystal growth system for growing crystalline material, the crystalline material including silicon carbide, includes a seed holder configured to hold a silicon carbide seed crystal. The seed crystal provides a growth surface for growth of the silicon carbide crystalline material. The system includes a crucible at least partially defining a crystal growth chamber. The system includes a source material. The system includes one or more baffles within the crystal growth chamber and spaced apart from the source material. The one or more baffles include one or more apertures defined through the one or more baffles. The baffle includes a long dimension that is non-perpendicular to the growth surface of the seed crystal.

Crystal growth systems for growing crystalline material comprising silicon carbide are provided. In one example, the crystal growth system includes a crucible at least partially defining a crystal growth chamber. The crystal growth chamber has a plurality of zones, each zone associated with a different processing profile. The system includes a silicon carbide crystal. The system includes a source material.

The invention discloses self-repairing and rapid-repairing cement-based mortar and a preparation method thereof, and belongs to the technical field of building materials. The self-repairing and rapid-repairing cement-based mortar is prepared from the following raw materials: 5500-6500 parts of a composite cementing material; 200 to 650 parts of an inorganic permeable crystalline material; 1500 to 3500 parts of a filling material; 307 to 510 parts of a rapid hardening component; 2-5 parts of a moisturizing and thickening component; 150 to 250 parts of a toughening and softening component; and 6-10 parts of a water reducing agent. The preparation method of the self-repairing and rapid-repairing cement-based mortar comprises the following steps: preparing the raw materials according to the proportion, uniformly mixing, adding the mixing water, and uniformly mixing to obtain the self-repairing and rapid-repairing cement-based mortar. The self-repairing quick-repairing cement-based mortar is efficient in water resistance and leaking stoppage, quick in setting and hardening and high in hour strength and has the function of silt; and a good self-repairing capability is achieved for microcosmic cracks of 0.1 mm.

Systems and methods for defect mitigation in silicon carbide crystal growth systems are provided. In an aspect, an example method includes providing a crystalline material in a first zone of the crystal growth chamber. In some implementations, the example method includes providing a silicon carbide vapor source material in a second zone of the crystal growth chamber. The example method includes providing an etching agent in the crystal growth chamber. The example method includes controlling a temperature gradient in the crystal growth chamber such that a first temperature in the first zone is greater than a second temperature in the second zone to implement an etching process on the crystalline material in the crystal growth chamber.

The invention relates to the technical field of metal organic framework materials (MOF) and isotope separation, in particular to a functionalized metal organic framework material for water / heavy water separation and a preparation method and application thereof. The metal organic framework material is a porous crystal material which is formed by coordination self-assembly of metal ions and V-shaped organic ligands and has a periodic network structure; the V-shaped organic ligand is a V-shaped dicarboxylic acid organic ligand modified by an oxygen-containing functional group designed through topological functionalization. According to the metal organic framework material, through topological functional design of a V-shaped organic ligand, a space confinement channel and a high-density oxygen active site are integrated in the same MOF material, and an ideal model system is provided for identification of water isotopes; according to the metal organic framework material, the framework structure flexibility, the pore channel confinement effect and the molecular recognition capability can be synergistically regulated and controlled, so that efficient recognition and separation of water / heavy water are realized.

The invention discloses a polyacid-based metal viologen framework crystalline material as well as a preparation method and application thereof, and belongs to the technical field of heterogeneous catalytic materials. The crystalline material is synthesized in one step through a hydrothermal method, the molecular formula is Cu2 (H2O) 2 (L) 2 [PW12O40] [OH]. 2H2O, the crystalline material belongs to a monoclinic system, the space group is P21, the cell parameters are alpha = 90 degrees, beta = 114.208 (2) degrees and gamma = 90 degrees, and the structure of the crystalline material is determined through X-ray diffraction. According to the material, accurate compounding of polyacid clusters and metal viologen on the molecular level is achieved, an effective electron transmission channel is constructed, separation of photon-generated carriers is remarkably promoted, and excellent photocatalytic activity is shown. At the ambient temperature, the crystalline material can be used as a catalyst to efficiently degrade dye pollutants (such as methylene blue and rhodamine B) in a water body, the degradation rate within 60 minutes exceeds 90%, and the crystalline material has good cycle stability and structural durability.

This application relates to the field of functional crystalline material preparation and microfluidic application technology, specifically disclosing a method and product for preparing formate crystals using core-shell microcapsules, including the following steps: (1) dissolving a solid alkaline raw material in a formic acid solution to prepare reaction solution a; (2) separately conveying polymer solution A and polymer solution B with phase separation characteristics, and reaction solution a, so that they are mixed at the intersection of microchannels to prepare dispersed phase b, which is then introduced into the assembly zone for phase separation assembly to form core-shell microcapsules; (3) the core-shell microcapsules are crystallized in a continuous temperature-changing crystallization zone to form formate solid; (4) the formate solid is collected, washed and dried sequentially to obtain the target product; (5) the oil layer is continuously extracted and returned to the assembly zone for recycling. The formate crystals prepared in this application not only have a large particle size, but also exhibit good size uniformity and morphological repeatability, and have the advantages of high throughput, green environmental protection, and simple operation.

The application provides a ternary mixed metal organotin supertetrahedral chalcogenide cluster crystal state for resin catalysts and a synthesis method and application thereof. The chalcogenide cluster compound comprises at least a core and a periphery, the core comprises metal ions, and the periphery comprises organotin; the core and the periphery form a cluster structure; and the molecular general formula of the chalcogenide cluster compound is (RSn)4M4M'2S 16 wherein R is selected from n-butyl (nBu) and / or phenyl (Ph); M is selected from In or Ga; and M' is selected from Zn, Cd, Mn and Co. The synthesis method of the application has low requirements on the purity of raw materials, simple process, and the crystal state is easy to repeat, convenient for production. The yield of the chalcogenide cluster crystal state obtained by the synthesis method of the application can reach more than 45%. The chalcogenide cluster compound of the application can be used in the fields of photoelectric catalysis and nonlinear optics.

A toner comprising a toner particle comprising a binder resin, a crystalline material, and a silica particle, wherein a number average particle diameter D1 of the silica particle comprised in the toner particle is 400 to 3000 nm; the silica particle has a pointed portion; and the crystalline material comprises a compound having an ester group.

The present invention relates to crystalline solids comprising organic molecules and to the use of the crystalline materials in optical films and electro-optical devices.

A computer implemented method of characterising a crystalline material is disclosed. The method includes obtaining diffraction data and a predicted phase distribution from a crystalline material. Modified Rietveld refinement is performed on the diffraction data. This includes i) determining an R-weighted pattern value, Rwp, and an R-expected value, Re, for a structural model of the crystalline material and ii) determining a goodness-of-fit value based on Rwp, Re and a likelihood estimator for the structural model. The goodness-of-fit value is optimised by repeating steps i) and ii) for different structural models of the crystalline material. An optimised structural model that provides an optimised goodness- of-fit value is obtained and the method outputs a characterisation of the crystalline material based on the obtained optimised structural model. The likelihood estimator is based on the predicted phase distribution of the crystalline material and a measured phase distribution, which is based on the structural model.

The invention discloses a circularly polarized light-emitting supramolecular self-assembly crystalline material as well as a preparation method and application of the circularly polarized light-emitting supramolecular self-assembly crystalline material. The supramolecular assembly crystalline material comprises a three-dimensional structure, and the three-dimensional structure is connected through a hydrogen bond formed between a hydrogen atom in a chiral secondary structure unit and an oxygen atom in a sulfonic acid group of 4, 4 '-bis (2-sulfostyryl) biphenyl disodium CBS. The crystalline material disclosed by the invention shows excellent chiral optical properties, good solvent stability and a remarkable luminous asymmetric factor; the circularly polarized light-emitting film material prepared from the material can effectively realize transmission and amplification of crystal optical performance.

The invention relates to a composite structure comprising: - a seed layer of single-crystal III-V composite material extending in a principal plane, - a support substrate of crystalline material, on which the seed layer is deposited via a bonding interface, the support substrate comprising a peripheral rim devoid of a seed layer, the peripheral rim extending around an edge of the seed layer in the principal plane, - an intermediate layer of amorphous material, disposed between the seed layer and the support substrate and present on the peripheral rim, - at least one trench present in the peripheral rim, extending, along an axis normal to the principal plane, through the intermediate layer to the support substrate, or even into the support substrate, the trench being located less than 100 micrometers from the edge in the principal plane. The invention also relates to a method for manufacturing said structure.Figure to be published with the abbreviation: -.

There is described a method of manufacturing a substrate for an optoelectronic device. The method has the steps of: supporting a first layer of a first crystalline material on a second layer of a second crystalline material different from said first crystalline material thereby exposing crystalline defects at a surface of said first layer; etching said first layer using first etching conditions, at least some of said crystalline defects expanding into pores running from said surface of the first layer towards said second layer; and heating said first and second layers up to a first temperature for a first period of time within a given environment, said heating transforming said pores into nanovoids attracting at least some of said crystalline defects away from said surface. In some embodiments, the method has a step of reheating the layers or a step of forming a pore containing region within the first layer.

A quantum computing device includes an optical resonator having a resonant wavelength band. A crystalline material including a crystal defect is contained within the optical resonator. The crystal defect has a ground state and an excited state, which has an emission wavelength in the resonant wavelength band. A source electrode and a drain electrode are disposed on opposing sides of the crystal defect and configured to apply a first electric field in the crystalline material along a longitudinal axis. A gate electrode is disposed in proximity to the crystal defect and configured to apply to the crystalline material a second electric field transverse to the longitudinal axis. Control circuitry is configured to apply a first voltage between the source and drain electrodes to control a charge state of the crystal defect and to apply a second voltage to the gate electrode to tune the emission wavelength.

The present invention relates to methods for preparing organic crystals based on precursor solutions containing organic molecules, to crystalline solids obtained from the methods and to the use of the crystalline materials in optical films and electro-optical devices.

This invention discloses a polyimide film and its preparation method. The polyimide film is a crystalline material with grains oriented along directions parallel to the film surface plane. Specifically, the crystal orientation factor in the MD direction is 0.08–0.65, and the crystal orientation factor in the TD direction is also 0.08–0.65. The polyimide film exhibits a dielectric constant less than or equal to 3.1 at 10 GHz, a dielectric loss less than or equal to 0.010 at 10 GHz, a dielectric constant less than or equal to 3.1 at 30 GHz, and a dielectric loss less than or equal to 0.012 at 30 GHz. The polyimide film possesses characteristics such as low dielectric constant, low dielectric loss, and low moisture absorption, and the crystal orientation in the MD / TD directions is individually controllable.

The invention relates to the technical field of photoelectrocatalysis, in particular to a Co (II) coordination polymer photoelectrode crystalline material and a preparation method and application thereof. The Co (II) coordination polymer {[Co (H2O) (Br-BDC) (BMIP)]. H2O} n is obtained from organic ligands BMIP, H2 (Br-BDC) and cobalt salt through a solvothermal method, cobalt (II) ions serve as three connection nodes, BMIP and H2 (Br-BDC) ligands serve as bridging ligands to be in mutual bridging, a two-dimensional honeycomb structure is formed, and a three-dimensional supramolecular structure is formed between layers through intermolecular hydrogen-bond interaction and pi-pi stacking. Wherein H2 (Br-BDC) is 2, 5-dibromoterephthalic acid, BMIP is 1, 3-bis (dimethylimidazolyl) propane, and n is a positive integer. The Co (II) coordination polymer shows relatively good photoelectric property, has the potential of serving as a photoelectrode material, has good optical and electrical characteristics, can be used for constructing an efficient photoelectrocatalysis water decomposition system, and has an application prospect in the aspects of photoelectric hydrolysis water oxidation and the like.

This invention discloses a discrete element method, system, medium, and equipment for simulating equivalent crystalline materials, relating to the field of numerical simulation of rock mechanics. The method includes: converting granite images into binary images using a binarization method to identify various minerals within the binary images; determining the size data of various minerals in the binary images based on a particle size statistical algorithm; extracting micromechanical parameters using nanoindentation experiments combined with a trial-and-error method, and constructing multiple sets of equivalent crystalline models based on the mineral size data; dividing each set of equivalent crystalline models into multiple regions using a Brazilian splitting experiment; determining the optimal magnification for each region of each set of equivalent crystalline models by magnifying from non-critical regions to critical regions using a magnification algorithm, obtaining differentiated equivalent crystalline models; and performing Brazilian splitting numerical simulation using these differentiated equivalent crystalline models to obtain simulation results.

This invention provides a method for removing a portion of a crystalline material (e.g., SiC) substrate. [Solution] The method involves bonding the surface of a substrate 172 to a rigid support 176 (for example, with a thickness of >800 μm). A subsurface laser-damaged region 173 is provided at a certain depth relative to the surface within the substrate. The substrate may be bonded to the support 176 by an adhesive material 174 having a glass transition temperature greater than 25°C. The crystalline material is fractured along the subsurface laser-damaged region 173 to create a bonded assembly comprising the support and a portion of the crystalline material. The fracture of the crystalline material is facilitated by (i) applying a mechanical force in close proximity to at least one support edge to impart a bending moment to the support, (ii) cooling the support if the support has a larger coefficient of thermal expansion than the crystalline material, and / or (iii) applying ultrasonic energy to the crystalline material.

The invention discloses a carbon material rich in intrinsic defects as well as a preparation method and application thereof, and belongs to the technical field of catalysts, fullerene or fullerene derivative carbon cages adopted by the invention have a pi conjugated structure, so that relatively strong pi-pi interaction force exists among molecules. Fullerene or a fullerene derivative is used as a raw material, a macroscopic crystalline material, namely a fullerene condensed state precursor, is obtained through self-assembly based on intermolecular acting force, the fullerene condensed state precursor is subjected to pre-etching treatment through oxygen plasma, surface modification is conducted on the fullerene condensed state precursor, and the fullerene or fullerene derivative is obtained. The preparation method comprises the following steps: preparing a fullerene condensed state precursor, performing two-stage temperature programming heat treatment of low-temperature pre-etching treatment and high-temperature roasting in ZnCl2 molten salt, endowing the fullerene condensed state precursor with five-membered ring topological defects and carbon intrinsic defects of boundaries and curvatures, so as to obtain the carbon material rich in intrinsic defects, and endowing the carbon material with good electro-catalytic performance by the intrinsic defect sites.

To provide an interconnect structure capable of reducing or preventing deterioration of electrical characteristics while reducing the size of the interconnect structure.SOLUTION: The interconnect structure and the integrated circuit device include a lower film including a non-single crystalline material and a ruthenium film located on the lower film and including a plurality of grains, wherein a texturing coefficient (F001) of the grains having a <001> orientation in the ruthenium film is 0.70 to 1, and an average grain size of the ruthenium film is 50 nm to 200 nm.SELECTED DRAWING: Figure 1

The application provides an ultramicroporous zinc-based MOF material, a preparation method thereof and application thereof in ammonia adsorption, and belongs to the technical field of crystalline materials. The material is an ultramicroporous zinc-based metal organic framework material with a three-dimensional periodic network structure, which is formed by coordination self-assembly of Zn 2+ ions, squarate ligands and triazoles ligands, wherein Zn 2+ ions exist in two coordination modes of hexa-coordinated octahedron and tetra-coordinated tetrahedron; the molecular formula of the material is [Zn2(C4O4)(C2H2N3)2], wherein C4O4 2‑ is a squarate ligand, and C2H2N3 ‑ is a triazole ligand. The application also provides application of the ultramicroporous zinc-based MOF material in ammonia adsorption. The MOF material has good stability, can maintain the integrity of the framework structure after being soaked in water for 7 days, and has good ammonia adsorption performance.

The disclosure is directed to cocrystals of fasoracetam, including R-fasoracetam, and various coformers. Crystalline materials comprising fasoracetam, including R-fasoracetam, are also provided. The disclosure further includes pharmaceutical compositions and methods of treatment of the cocrystals and crystalline materials of the disclosure.

The invention relates to a niobium tantalum oxyfluoride acid ammonium salt second-order nonlinear optical crystalline material and preparation and application thereof, the chemical formula of the material is (NH4) 5 (NbOF4) (TaF7) 2, the crystalline material belongs to a tetragonal system, the space group is I4cm, and the cell parameters are alpha = beta = gamma = 90 degrees and Z = 2. Under 1064nm laser irradiation, the powder frequency-doubled effect of the nonlinear optical crystal (NH4) 5 (NbOF4) (TaF7) 2 can reach 3.5 times that of a KH2PO4 (KDP) crystal, under 532nm laser irradiation, the powder frequency-doubled effect of the nonlinear optical crystal (NH4) 5 (NbOF4) (TaF7) 2 is 0.35 times that of a beta-BaB2O4 (BBO) crystal, and phase matching can be realized. In addition, the ultraviolet absorption cutoff edge of the crystalline material is less than 195 nm, and the crystalline material shows moderate birefringence (0.095 at-546 nm). The crystalline material provided by the invention has important application value in the photoelectric fields of solid-state lasers, spectral analysis, precision manufacturing, optical communication and the like.

The present application relates to the technical field of tunnel drainage, in particular to a kind of tunnel longitudinal drainage pipeline dredging device, including fixed seat, fixed seat upper portion is equipped with fixed mechanism, fixed seat inside bottom surface one side is fixedly provided with motor, motor front is equipped with dredging mechanism, dredging mechanism includes multiple rotating shafts, which are linearly and equidistantly arranged, one of the rotating shafts has a moving seat in the middle, the moving seat is a circular table structure with a smaller front and a larger back, and is coaxial with the rotating shaft, the moving seat and the fixed seat are located on the same axis, the dredging mechanism further includes a turntable, the turntable is coaxially and slidingly connected to the rotating shaft, and multiple first breaking blades are fixedly arranged on the turntable in a ring-shaped and equidistant manner. The present application is provided with a drill bit, which can remove the crystalline material on the inner wall of the drainage pipeline from the vertical direction by cooperating with the driving structure in the dredging mechanism. In cooperation with the other cleaning structures on the turntable and the moving seat, the device can fully dredge and clean the drainage pipeline without damaging the surrounding mountain structure and the ecological environment.

A method of forming a ceramic matrix composite includes arranging a plurality of fibers into a preform, each of the plurality of fibers being formed from silicon carbide, depositing a nucleating layer on the plurality of fibers, the nucleating layer comprising a crystalline material having an a-lattice constant and a c-lattice constant, and depositing a boron nitride layer on the nucleating layer. The c-lattice constant of the crystalline material of the nucleating layer corresponds to an a-lattice constant of the silicon carbide, such that the c-lattice constant of the crystalline material is within 3.0% of the a-lattice constant of the silicon carbide.

The invention provides desulfurization solution erosion resistant concrete and a preparation method thereof. The desulfurization solution erosion resistant concrete is suitable for coke oven gas desulfurization solution alkaline and various composite salt ion erosion environments. The concrete is formed by compounding water, cement, fly ash, superfine slag powder, a capillary crystalline material, limestone coarse aggregate, limestone fine aggregate and a polycarboxylate water reducing agent according to a preset weight part ratio, the selection of the limestone aggregate ensures the stability of the aggregate structure in alkaline and salty erosion environments, and the synergistic effect of fly ash and superfine slag powder in the admixture ensures the stability of the aggregate structure in the alkaline and salty erosion environments. The compactness and the composite salt corrosion resistance of the concrete are improved, and the composite salt ion penetration resistance is enhanced through internal doping of the capillary crystalline material. According to the preparation method, the concrete with stable performance is obtained by premixing part of the cement and the capillary crystalline material, sequentially mixing and performing standard curing. The durability and the service life of the concrete under the erosion condition of the coke oven gas desulfurization liquid are remarkably improved, the environmental pollution is reduced, and good economic benefits and application prospects are achieved.

An insertion tool for inserting at least a portion of a medical device into a subject, an insertion device including the insertion tool and an insertion mechanism, and a method for manufacturing the insertion tool, wherein the insertion tool includes an entry portion including a composite material, the composite material including at least one first material and at least one second material, the first material being an amorphous material or an amorphous composite, and the second material being a fibrillar material or a fibrillar composite or a crystalline material or a crystalline composite, wherein the fluid absorbency of the first material of the composite material is higher than the fluid absorbency of the second material of the composite material, and the insertion device is adapted to soften upon contact with bodily fluids due to the fluid absorbency of at least the amorphous material or the amorphous composite.