Negative electrode for lithium secondary battery and lithium secondary battery including the negative electrode
A negative electrode and negative electrode active material technology, applied in the direction of secondary batteries, battery electrodes, negative electrodes, etc., can solve the problems of low conductivity of silicon-based negative electrodes, achieve high conductivity, reduce irreversible capacity, and high energy density.
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Embodiment 1
[0087] The silicon oxide-based composite core forming the first negative electrode active material was prepared as follows. Powdered Si and SiO 2 Mixed in a 1:1 ratio (molar ratio) and heat-treated under a reduced pressure of 1 Torr to evaporate the mixture to SiO x (0x (02 The evaporation temperature of Mg is 1400 °C, and the evaporation temperature of Mg is 900 °C. The deposited product is Mg-SiO x (xx crushed to diameter (D 50 ) is about 5 μm.
[0088] To form a carbon coating covering the core of the silica-based composite, the Mg-SiO x The chamber was introduced and supplied with methane gas under an argon atmosphere to form a carbon coating by chemical vapor deposition (CVD) at 950°C. The thickness of the carbon coating was determined to be 40 nm as determined by transmission electron microscopy (TEM) analysis. In this way, the first anode active material was obtained. The silicon oxide-based composite includes: i) Si; ii) composed of the chemical formula SiO x (...
Embodiment 2
[0096] A coin-type secondary half cell was obtained in the same manner as in Example 1, except that the first negative electrode active material and the second negative electrode active material were used in a weight ratio of 10:90.
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