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A kind of base treatment agent and preparation method thereof

A technology of base treatment agent and dispersant, which is applied in the field of base treatment agent and its preparation to achieve excellent low-temperature applicability and good storage stability

Active Publication Date: 2021-11-19
杭州东方雨虹建筑材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] Although solvent-based and water-based base treatment agents have been widely used for different base conditions, for water-based bases that must be applied at low temperatures below 0°C (as low as -5°C) and have high adhesion Treatment agent, the storage stability of 10 days under standard conditions is less than 1%. There is no water-based base treatment agent product on the market that meets the above requirements

Method used

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  • A kind of base treatment agent and preparation method thereof

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preparation example Construction

[0027] The preparation method of the adhesive joint agent can be carried out with reference to the prior art. Preferably, the preparation method of the adhesive joint agent comprises: 1) 80 parts of 10wt% PVA aqueous solution, 8 parts of water glass and 20 parts of water are mixed at 60° C. Mix well; 2) Slowly add 0.2g of TO-7 emulsifier and mix evenly, then add 1.0g of 30wt% citric acid aqueous solution dropwise and mix evenly; 3) Stir and emulsify at 80°C for 20min; 4 ) Finally, mix 4 parts of water glass and 10 parts of water evenly, add slowly drop by drop, and ripen for 24 hours to prepare the adhesive joint agent.

[0028] In the present invention, the DOP plasticizer can make the base treatment agent have a wider temperature application range, specifically, improve the low temperature applicability, and can reduce the construction temperature to below 0°C, and the lowest can reach -5°C. The DOP plasticizer is dioctyl phthalate, referred to as dioctyl phthalate, which is...

Embodiment 1

[0054] Add 22 parts of 90# petroleum asphalt and 2 parts of naphthenic oil into a high-speed mixer, and stir at 600 rpm for 15 minutes at a temperature of 140°C to obtain mixture A; heat 65 parts of water to 60°C, and add iso 0.5 parts of alcohol TO-7 nonionic emulsifier, stirred at 700rpm for 30min to obtain a soap solution; added the soap solution to a high-speed mixer and mixed with mixture A, and stirred at a temperature of 80°C for 30min at a rotation speed of 800rpm to obtain a mixture C; add mixture C to a colloid mill and grind for 10 minutes to obtain emulsified asphalt; heat 4 parts of adhesive joint agent to 50 ° C, add 2 parts of DOP plasticizer to it, and stir at a speed of 500 rpm for 25 minutes to obtain mixture B; Add mixture B, 0.1 part of UV-571 homogeneous regulator to the emulsified asphalt, and stir at a speed of 1000 rpm for 20 minutes under high-speed stirring conditions; then add 0.4 parts of TY-5110 dispersant and calcium carbonate additive to the high-...

Embodiment 2

[0056] Add 20 parts of 90# petroleum asphalt and 3 parts of white wax base oil into a high-speed mixer, and stir at 600 rpm for 15 minutes at a temperature of 140°C to obtain mixture A; heat 70 parts of water to 60°C, and add isomer 0.6 parts of alcohol ether XL-90 nonionic emulsifier, stirred at 700rpm for 30min to obtain soap liquid; added soap liquid to a high-speed mixer and mixed with mixture A, and stirred at 80°C for 30min at 800rpm to obtain a mixture C; Add mixture C to a colloid mill and grind for 10 minutes to obtain emulsified asphalt; heat 3 parts of adhesive joint agent to 50 ° C, add 1 part of DOP plasticizer to it, and stir at a speed of 500 rpm for 25 minutes to obtain mixture B; Add mixture B and 0.1 part of R218 homogeneous conditioner to the emulsified asphalt, and stir at a speed of 1000 rpm for 20 minutes under high-speed stirring conditions; then add 0.3 parts of TY-5110 dispersant and 2 parts of calcium carbonate additive to the high-speed mixer in turn ...

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Abstract

The invention belongs to the technical field of waterproof materials for construction projects, and discloses a base layer treatment agent and a preparation method thereof. The base layer treatment agent is prepared from the following raw materials by mass percentage: 10-61% of asphalt, 1-13% of softening oil, Water 50‑70%, Emulsifier 0.1‑1.7%, Adhesive Joint Agent 3‑10%, DOP Plasticizer 1‑13%, Homogeneous Regulator 0.05‑2.1%, Dispersant 0.01‑0.5%, Additive 1‑ 11%. The base layer treatment agent of the present invention has excellent low temperature applicability, high-strength bonding performance, good storage stability, can maintain a good construction and application state at temperatures above -5°C, and the bonding strength of the figure-eight mold can reach more than 0.9 MPa. The peel strength of the coil after bonding can reach more than 2.0MPa, and the storage stability is less than 1% after being placed under standard conditions for 10 days.

Description

technical field [0001] The invention belongs to the technical field of construction engineering waterproof materials, and more specifically relates to a base treatment agent and a preparation method thereof. Background technique [0002] The base treatment agent is a kind of coating used to seal the base and enhance the adhesion between the base and the membrane during the construction of waterproof coiled materials. It is divided into two categories: solvent-based and water-based. Solvent-based base treatment agent has good permeability and adhesion, but it is not suitable for use on wet base surfaces. At the same time, it is harmful to human body and environment during construction, and it is dangerous and flammable. Water-based base treatment agent can be used on wet base surface, but it can’t be used at low temperature (generally above 5°C), its adhesion is slightly poor, and it is less harmful to human body and environment. At present, because the base treatment agent ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D195/00C09D7/61C09D7/63C09D7/20
CPCC08K2003/265C09D195/00C09D7/20C09D7/61C09D7/63C08K13/02C08K3/26C08K5/12
Inventor 白福平陈晓文李善法吴士玮侯建伟
Owner 杭州东方雨虹建筑材料有限公司