A kind of preparation method of impregnated film paper decoration formaldehyde-free wood-based panel
A technology of impregnating adhesive film paper and wood-based panels, which is applied in the jointing of wooden veneers, papermaking, paper, etc., to achieve the effect of increasing the amount of glue hanging and improving the scratch resistance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0030] 1) Add polyethylene glycol (molecular weight 200) and isophorone diisocyanate into a reaction kettle with a stirring and reflux device according to a molar ratio of 0.8, and carry out a prepolymerization reaction under the protection of high-purity nitrogen. The temperature is 40°C, and the reaction time is 1h to obtain a polyurethane prepolymer.
[0031] 2) The temperature of the prepolymer was raised to 65° C., and 1,4-butanediol was added dropwise to the prepolymer for 20 minutes. The chain extension reaction lasted 1.5 hours, and the stirring speed was 50 r / min. Then the temperature was lowered to 40°C, and the hydrophilic agent was added, and the addition was completed within 30 minutes, and the reaction time of this step was 0.5 hours.
[0032] 3) Cool to room temperature, add glacial acetic acid for neutralization, and reduce viscosity with appropriate amount of acetone. After the viscosity is suitable, add water and high-speed shearing. The shearing speed is 200...
Embodiment 2
[0041] 1) Add polyester diol CMA-1024 and isophorone diisocyanate into a reaction kettle with a stirring and reflux device according to a molar ratio of 2, and carry out a prepolymerization reaction under the protection of high-purity nitrogen, and the reaction temperature The temperature is 60°C, the reaction time is 0.5h, and the polyurethane prepolymer is obtained.
[0042] 2) The temperature of the prepolymer was raised to 80°C, and ethylene glycol was added dropwise to the prepolymer for 10 min, the chain extension reaction time was 0.5 h, and the stirring speed was 100 r / min. Then the temperature was lowered to 60°C, and the hydrophilic agent was added, and the addition was completed within 30 minutes, and the reaction time of this step was 1.5 hours.
[0043] 3) Cool to room temperature, add glacial acetic acid for neutralization, and reduce viscosity with appropriate amount of acetone. After the viscosity is suitable, add water and high-speed shearing at a shearing spe...
Embodiment 3
[0052] 1) Add polyester diol CMA-1024, Polyethylene Glycol (both molar ratio 1: 1) and hexamethylene diisocyanate into the reactor with stirring and reflux device according to molar ratio 1.3, in Under the protection of high-purity nitrogen, a prepolymerization reaction was carried out at a reaction temperature of 50° C. and a reaction time of 0.7 h to obtain a polyurethane prepolymer.
[0053] 2) The temperature of the prepolymer was raised to 75° C., and propylene glycol was added dropwise to the prepolymer for 15 minutes, the chain extension reaction time was 0.8 hours, and the stirring speed was 80 r / min. Then the temperature was lowered to 50°C, and the hydrophilic agent was added, and the addition was completed within 30 minutes, and the reaction time of this step was 1 hour.
[0054] 3) Cool to room temperature, add glacial acetic acid for neutralization, and reduce viscosity with appropriate amount of acetone. After the viscosity is suitable, add water and high-speed s...
PUM
Property | Measurement | Unit |
---|---|---|
particle diameter | aaaaa | aaaaa |
particle diameter | aaaaa | aaaaa |
particle diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com