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A targeted refinement of Amla emblica, its preparation method and its application in cigarettes

An emblica and targeted technology, which is applied in the field of cigarette flavors and fragrances, can solve the problems of large differences, complex types of ingredients, and unremarkable cigarette functions, and achieve the effects of outstanding functionality, improved sensory quality, and delicate smoke

Active Publication Date: 2022-05-03
CHINA TOBACCO SICHUAN IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The types of components contained in the extract of Amla emblica are relatively complex, with large differences, and their functions in cigarette applications are not prominent, so they are rarely used in tobacco flavor raw materials

Method used

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  • A targeted refinement of Amla emblica, its preparation method and its application in cigarettes
  • A targeted refinement of Amla emblica, its preparation method and its application in cigarettes
  • A targeted refinement of Amla emblica, its preparation method and its application in cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Weigh 50g of dry emblica, add 500g of pure water after crushing, heat in a water bath at 90°C to condense and reflux for extraction 3 times, each time for 2h, combine the filtrates 3 times, concentrate under reduced pressure to 50g of crude extract (code A), and after cooling Add 200g of 95% ethanol for alcohol precipitation. After standing for 24 hours, centrifuge to remove the precipitate. The supernatant is concentrated under reduced pressure until it has no ethanol smell, and diluted to 30g with pure water to obtain the polysaccharide-removed emblica extract (code A1). The polysaccharide-removed emblica extract was adsorbed by the macroporous adsorption resin AB-8 for 24 hours, and the sample was loaded according to the ratio of the crude drug amount to the resin amount at 1:10. After the adsorption was completed, 4BV was eluted with pure water, and the pure water eluate was collected to reduce Concentrated under pressure and then dried to obtain the targeted refined...

Embodiment 2

[0031] Weigh 11kg of dry emblica, add 110kg of pure water after crushing, heat at 90°C to extract 3 times, each time for 2h, combine the filtrates 3 times, concentrate under reduced pressure to 1kg of crude extract (code B), add 4kg of 95% Ethanol was used for alcohol precipitation, and after standing for 24 hours, the precipitate was removed by centrifugation, and the supernatant was concentrated under reduced pressure until it had no ethanol smell, and 4.58 kg of emblica extract (code B1) from which polysaccharides were removed was obtained. Weigh 333g of emblica extract (crude drug amount 800g) from which polysaccharides have been removed, and absorb it through the macroporous adsorption resin AB-8 for 24 hours, load the sample according to the ratio of crude drug amount and resin amount 1:10, and elute 8BV with pure water after the adsorption is completed. The pure water eluate was collected, concentrated under reduced pressure, and then dried to obtain the targeted refined...

Embodiment 3

[0038] The polysaccharide-removed emblica extract and emblica targeted refined product in Example 1 were dissolved and diluted with 10% ethanol respectively, and the diluted solution was sprayed on the sample shredded tobacco 3#, and the dosage of emblica targeted refined product was 0.05% by weight of shredded tobacco, sealed and stored for 24 hours, rolled into cigarettes.

[0039] The results of sensory evaluation showed that: compared with the cigarette samples added with polysaccharide-removed emblica extract, the cigarette samples added with emblica targeted refinement had lively, soft, transparent smoke and increased roundness, which was significantly better than Before refining.

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Abstract

The invention discloses a targeted refined product of Amla emblica, a preparation method and its application in cigarettes, and relates to the technical field of cigarette flavor and fragrance. After sinking, use macroporous adsorption resin to separate, collect the pure water eluate, and obtain the targeted refined product of Amla emblica. The refined product can be used in shredded tobacco, tobacco stems and tobacco flakes of cigarettes. The greatest feature of the present invention is that the refined emblica raw material is effectively enriched with organic acids, phenolic acids, and some sugars, increasing the content of functional components; In terms of fine smoke, pungent reduction and sweetening, the functionality is more prominent and has been significantly improved, improving the comfort and sensory quality of cigarette smoking.

Description

technical field [0001] The invention relates to the technical field of cigarette flavors and fragrances, in particular to a targeted refined product of emblica emblica, a preparation method and its application in cigarettes. Background technique [0002] Natural tobacco flavor materials derived from fruits, such as apricots, plums, figs, raisins, etc., occupy an important position in the application of cigarettes because they are rich in organic acids and sugars. Adding organic acids to cigarettes can adjust the ratio of protonated and free nicotine in the smoke during the cigarette smoking process, making the smoke taste mellow, reducing the irritation of flue-cured tobacco, increasing the smoke concentration, and improving the cigarette smoking. Sensory comfort plays an important role. The sweetness or sweetness of cigarette smoking can bring comfort and pleasure. Therefore, the use of fruit-like natural flavoring materials in cigarettes can effectively increase the swee...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/30
CPCA24B15/303
Inventor 叶烨李东亮耿宗泽
Owner CHINA TOBACCO SICHUAN IND CO LTD
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