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A kind of processing technology of safflower decoction pieces

A processing technology, safflower technology, applied to medical preparations containing active ingredients, pharmaceutical formulas, non-central analgesics, etc., can solve oxidative degradation or volatilization, reduction of safflower efficacy, loss of multiple active ingredients, etc. problem, to achieve the effect of increasing the content of active ingredients, increasing the content of active ingredients for promoting blood circulation, and reducing the loss of active ingredients

Active Publication Date: 2022-02-15
安徽鑫泰药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The processing methods of safflower decoction pieces mainly include drying, slightly frying, charcoal frying, vinegar broiling, etc. However, no matter which method is used, heating and drying are required. During the heating process, various active ingredients will inevitably suffer losses, resulting in redness. Potency of flowers reduced
During the storage of the finished safflower decoction pieces, the active ingredients will be oxidatively degraded or volatilized over time, which will also lead to a decrease in the efficacy of safflower

Method used

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  • A kind of processing technology of safflower decoction pieces
  • A kind of processing technology of safflower decoction pieces

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Embodiment 1: prepare a kind of safflower decoction piece as follows, concrete steps are as follows:

[0023] (1) Remove the sepals from newly harvested safflower and dry them to obtain dried safflower;

[0024] The dry product of safflower is moistened with the enhancing solution for 12 hours, and then freeze-dried to obtain the dry product 2. The weight ratio of the dried product of the safflower and the moisturizing enhancing solution is 1:5-8. The preparation method of the enhancing liquid is as follows:

[0025] (A) The dried safflower was boiled with water at a weight ratio of 1:10, and the oily volatile liquid was extracted by steam reflux extraction; the extraction solvent was pure water; the temperature was 60°C; the extraction was done once, 10 minutes each time.

[0026] (B) After the extraction is completed, filter the remaining aqueous solution to remove the residue, and use the macroporous resin H to filter the filtrate 103 Carry out the extraction of sa...

Embodiment 2

[0029] Embodiment 2: prepare a kind of safflower decoction piece as follows, concrete steps are as follows:

[0030] (1) Remove the sepals from newly harvested safflower and dry them to obtain dried safflower;

[0031] (2) Moisten the dried safflower with the enhancing solution for 12 hours, and freeze-dry to obtain the dry product 2. The weight ratio of the dried safflower to the enhancing solution is 1:8. The preparation method of the enhancing liquid is as follows:

[0032] (A) 20 parts by weight of Panax notoginseng, 10 parts by weight of Motherwort, 10 parts by weight of Salvia miltiorrhiza, 20 parts by weight of Chuanxiong, 15 parts by weight of angelica, 25 parts by weight of paeonol, 5 parts by weight of raw cattail, 5 parts by weight of frankincense, 200 parts by weight After weighing and preparing a portion of safflower, add water to boil according to the weight ratio of material to liquid 1:20, and extract the oily volatile liquid by steam reflux extraction method;...

Embodiment 3

[0036] Embodiment 3: prepare a kind of safflower decoction piece as follows, concrete steps are as follows:

[0037] (1) Remove the sepals of the newly harvested safflower, and dry the dried safflower; moisten the dried safflower with the enhancing solution for 24 hours, and freeze-dry to obtain the second dried safflower. The weight ratio of liquid is 1:6.5. The preparation method of the enhancing liquid is as follows:

[0038] (A) Boil the dry safflower product with water according to the weight ratio of 1:15, and extract the oily volatile liquid by steam reflux extraction; the extraction solvent is acid water with pH=3; the temperature is 65°C; extract 3 times, each time 1h.

[0039] (B) After the extraction is completed, filter the remaining aqueous solution to remove the residue, and use the macroporous resin H to filter the filtrate 103 Carry out the extraction of safflower yellow, the ratio of the amount of sample on the column to the amount of resin is 1:10 (W:V), a...

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Abstract

The invention discloses a process for processing high-quality safflower decoction pieces, which relates to the technical field of preparation of safflower decoction pieces, including steps such as drying, moistening with enhancing liquid, freeze-drying, vinegar roasting, and wax sealing. Dried products can effectively increase the content of active ingredients in safflower semi-finished products, offset part of the loss during processing, and increase the active ingredient content in finished safflower decoction pieces. Insulate the air, reduce the loss of active ingredients in the safflower decoction pieces during storage, and improve the quality of the safflower decoction pieces in storage. Vinegar roasting can reduce the pH value of the aqueous solution of safflower decoction pieces, effectively increase the dissolution rate of safflower yellow pigment, and improve the efficacy of the medicine.

Description

technical field [0001] The invention relates to the field of preparation of safflower decoction pieces, in particular to a processing technology of safflower decoction pieces. Background technique [0002] The traditional Chinese medicine safflower is the dried flower of the Compositae plant safflower, also known as grass safflower. The chemical components obtained from safflower include flavonoids, alkaloids, polyynes, spermidine, lignans, sesquiterpenes, organic acids, sterols, alkyl glycols, volatile oils and polysaccharides, among which flavonoids Safflower yellow pigment is the main active ingredient. Safflower yellow is a water-soluble pigment, and its color changes with the pH of the solution. It is stable to light, heat and most metal ions, while polyacetylene compound aglycone is mostly in the form of oil and is relatively unstable. prone to fusion. The volatile oil is very easy to volatilize during long-term storage in the air or during processing, resulting in ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/286A61K36/88A61P29/00A61K133/00
CPCA61K36/286A61K36/258A61K36/533A61K36/537A61K36/236A61K36/232A61K36/71A61K36/65A61K36/88A61K36/324A61P29/00A61K2236/17A61K2236/10A61K2236/331A61K2236/37A61K2236/39A61K2236/53A61K2236/51A61K2236/55A61K2300/00
Inventor 宋学才祝涛
Owner 安徽鑫泰药业有限公司
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