Oxalic acid and genipin cross-linked hydrogel filter membrane and application thereof in molecular ion separation under high salinity
A molecular ion and genipin technology, applied in membrane separation, filtration membrane, functional materials, high-salinity wastewater treatment, hydrogel field, can solve the problems of poor stability and mechanical strength
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Embodiment 1
[0017] e) preparing an aqueous solution of a mixture of sodium alginate and 0.5% carboxymethyl chitosan at a mass percentage concentration of 1%, and standing for defoaming to obtain a casting solution;
[0018] f) preparing an aqueous solution of oxalic acid with a mass percent concentration of 1% as a crosslinking solution 1; preparing an aqueous solution of genipin with a mass percent concentration of 2% as a crosslinking solution 2;
[0019] g) Pour the casting solution obtained in step a) onto a dry and clean glass plate, scrape it flat with a glass rod with a diameter of 20 μm copper wires wound at both ends, and then immediately soak the glass plate and the scraped film into step b) The obtained cross-linking solution 1 was cross-linked for 5 minutes to obtain a preliminary cross-linked hydrogel film; the preliminary cross-linked hydrogel film was taken out, soaked in the cross-linking solution 2 obtained in step b) and cross-linked for 10 min. Fully wash the membrane w...
Embodiment 2
[0022] a) preparing an aqueous solution of a mixture of sodium alginate with a mass percentage concentration of 5% and 3.5% sericin, and standing for defoaming to obtain a casting solution;
[0023] b) preparing an aqueous solution of oxalic acid with a mass percentage concentration of 10% as crosslinking solution 1; preparing an aqueous solution of genipin with a mass percentage concentration of 0.01% as crosslinking solution 2;
[0024] c) Pour the film casting solution obtained in step a) onto a dry and clean glass plate, scrape it flat with a glass rod with a diameter of 1500 μm copper wire wound at both ends, and then immediately soak the glass plate and the scraped film into step b) The obtained cross-linking solution 1 was cross-linked for 600 min to obtain a preliminary cross-linked hydrogel film; the preliminary cross-linked hydrogel film was taken out, soaked in the cross-linking solution 2 obtained in step b) and cross-linked for 1800 min, and used to Fully wash the...
Embodiment 3
[0027] a) preparing an aqueous solution of a mixture of sodium alginate and 1% polyvinyl alcohol with a mass percentage concentration of 4%, and standing for defoaming to obtain a casting solution;
[0028] b) preparing an aqueous solution of oxalic acid with a mass percent concentration of 5% as a crosslinking solution 1; preparing an aqueous solution of genipin with a mass percent concentration of 1% as a crosslinking solution 2;
[0029]c) Pour the casting solution obtained in step a) onto a dry and clean glass plate, scrape it flat with a glass rod with a diameter of 100 μm copper wires wound at both ends, and then immediately soak the glass plate and the scraped film into step b) The obtained cross-linking solution 1 was cross-linked for 60 min to obtain a preliminary cross-linked hydrogel film; the preliminary cross-linked hydrogel film was taken out, soaked in the cross-linking solution 2 obtained in step b) for cross-linking for 60 min, and used to Fully wash the membr...
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Abstract
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