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Light adjusting mechanism of organic synthesis photoreaction experimental device

An experimental device and organic synthesis technology, applied in the field of chemical experimental devices, can solve problems such as the influence of experimental results and time-consuming multi-equipment

Active Publication Date: 2021-09-10
重庆新申世纪新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the prior art, PMW is usually used to regulate the light intensity of the lamp tube, and multiple experiments or different experiments are carried out in different devices at the same time to carry out experiments on the influence of light intensity on the photoreaction of organic synthesis, which requires more The equipment and time-consuming are long, and the mechanical error between different equipment will also affect the experimental results

Method used

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  • Light adjusting mechanism of organic synthesis photoreaction experimental device
  • Light adjusting mechanism of organic synthesis photoreaction experimental device
  • Light adjusting mechanism of organic synthesis photoreaction experimental device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] In Example 1, in different test tubes 7, a comparative experiment of organic synthesis photoreaction under different light intensities was carried out:

[0045] Put a plurality of test tubes 7 equipped with the same experimental product on the test tube holder assembly 5, drive the floating table 8 to move in the plane by adjusting the motor one 11 and the second motor 12, and adjust the distance between the lamp tube 3 and each test tube 7 according to the gradient. distance, so that different test tubes 7 receive different light intensities, cover the top cover 9 to prevent the interference of external light sources, turn on the lamp tube 3 and the rotation motor 52 so that each side of the test tube 7 is evenly illuminated, and turn off the lamp tube after reaching the specified time 3 and the rotation motor 52, detect the state of the product in each test tube 7, and can obtain the influence of different light intensities on the photoreaction of organic synthesis und...

Embodiment 2

[0046] In embodiment two, carry out organic synthesis photoreaction periodical illumination experiment:

[0047] Put one or more test tubes 7 with experimental products on the test tube holder assembly 5, drive the floating platform 8 to move in the plane by adjusting the motor one 11 and the two motors 12, adjust the lamp tube 3 to the test tube according to the cycle The nearest and the farthest distances of 7, cover the top cover 9 to prevent the interference of external light sources, turn on the lamp tube 3 and the rotation motor 52 so that each side of the test tube 7 is evenly illuminated, turn on the turntable motor 17 to make each test tube 7 go around the lamp tube 3. Periodically rotate the distance, turn off the lamp tube 3 and the rotation motor 52 after the specified time, and detect each test tube 7. By detecting the state of the product in the test tube 7 in different cycles for many times, the light source in different cycles can be obtained. Effects on photor...

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PUM

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Abstract

The invention discloses a light adjusting mechanism of an organic synthesis photoreaction experimental device. The light adjusting mechanism comprises a base and a lamp tube, the base is a cavity with an upper opening, a floating table capable of moving along the horizontal plane is arranged above the base, a vertical lamp tube is fixed in the middle of the floating table, a rotatable rotating ring is arranged between the inner wall of the base and the floating table, a plurality of test tube seat assemblies are circumferentially distributed on the rotating ring, and test tubes can be placed on the test tube seat assemblies; and the periphery of the test tube seat assembly on the base is surrounded by a shell, the shell is higher than the lamp tube and the test tube, and a detachable top cover is arranged above the shell. Compared with the prior art, the test tube can uniformly receive illumination of the lamp tube; when the rotating ring rotates and drives the floating table to rotate through a sliding rod, the central position of the floating table, namely the position of the lamp tube, is always kept unchanged, so that the test tube on the test tube base can rotate around the lamp tube, and the illumination intensity is periodically changed.

Description

technical field [0001] The invention relates to the technical field of a chemical experiment device, in particular to a light adjustment mechanism of an organic synthesis photoreaction experiment device. Background technique [0002] In a photochemical reaction, the reactant molecules absorb light energy, and the ground state of the reactant molecules transitions to an excited state, becoming an activated reactant molecule, and then a chemical reaction occurs. The energy absorbed by a molecule from the ground state to the excited state sometimes far exceeds the energy available for thermochemical reactions. Therefore, organic photochemical synthesis can accomplish many synthetic tasks that are difficult or even impossible for thermochemical reactions. [0003] The photochemical reaction is to make a certain group of the reactant excite the surface of the reactant to promote the reaction through the absorption of photons, and the energy of the reaction product can be higher ...

Claims

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Application Information

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IPC IPC(8): B01J19/12B01J19/28
CPCB01J19/122B01J19/28B01J19/0053
Inventor 申静王强龙俊华
Owner 重庆新申世纪新材料科技有限公司
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