Durable eyeliner gel pen and preparation method thereof
A persistent eyeliner technology, applied in the field of persistent eyeliner gel pen and its preparation, can solve problems such as line smearing and the like, and achieve the effects of soft touch, excellent coloring degree, bright and single color
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[0038] In addition, the perfluorooctyltriethoxysilane used in the above-mentioned toner and filling powder can preferably be modified perfluorooctyltriethoxysilane, and its preparation method includes the following steps:
[0039] (1) Miscanthus seed oil is dripped into the sodium alginate aqueous solution containing the first lipase at a rate of 100-500 μL / min, stirred and reacted at 50-70°C for 13-16 hours, and the pH is controlled to be 4-5, wherein , the mass ratio of mango flower seed oil to sodium alginate is 1:1.1~1.6, the first lipase is Thermophila pilosa lipase, H.insolens cutinase or C.antarctica lipase A; after the reaction is completed, it is distilled and removed by-product glycerol and glycerides;
[0040] (2) Heat and hydrolyze perfluorooctyltriethoxysilane at 80-100°C for 15-18 hours, add the resultant in step (1), the second lipase, and p-toluenesulfonic acid, React at 100°C for 5-10 hours, the mass ratio of perfluorooctyltriethoxysilane to the product in st...
Embodiment 1
[0044] The raw material of a long-lasting gel eyeliner includes the following components, the toner and the filler powder are treated with perfluorooctyltriethoxysilane (FL).
[0045] components Content in parts by weight / w% use CI 77499 / FL 20.5 Colorant Mica / FL 10 filler Boron nitride / FL 5 filler Polydimethylsiloxane 5.4 solvent Stearyl Dimethicone 8 Forming agent C30-45 Alkyl Dimethicone 12 Forming agent Polymethylsilsesquioxane 19 Film former Trimethylsiloxysilicate 10 Film former tocopheryl acetate 0.1 Antioxidants
[0046] Its preparation method comprises the following steps:
[0047] Treat the toner and filling powder with perfluorooctyltriethoxysilane; weigh stearyl dimethicone, C30-45 alkyl dimethicone, and tocopherol in the formula Heat and stir at 100°C after acetic acid ester, the rotation speed is 50rpm, keep stirring while adding the treated CI 77499; after grinding 7 times un...
Embodiment 2
[0049] The raw material of a long-lasting gel eyeliner includes the following components, the toner and the filler powder are treated with perfluorooctyltriethoxysilane (FL).
[0050] components Content in parts by weight / w% use CI 77499 / FL 20.5 Colorant Mica / FL 10 filler Boron nitride / FL 5 filler Polydimethylsiloxane 5.4 solvent Stearyl Dimethicone 8 Forming agent C30-45 Alkyl Dimethicone 12 Forming agent Polymethylsilsesquioxane 19 Film former Trimethylsiloxysilicate 10 Film former tocopheryl acetate 0.1 Antioxidants
[0051] Its preparation method comprises the following steps:
[0052] Treat the toner and filling powder with perfluorooctyltriethoxysilane; weigh stearyl dimethicone, C30-45 alkyl dimethicone, and tocopherol in the formula After acetate ester, heat and stir at 80°C, the rotation speed is 70rpm, keep stirring while adding the treated CI 77499; after grinding 5 times under ...
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