Medicine for treating wind-heat syndrome due to exopathy and preparation process thereof
A technology for wind-heat syndrome and medicine, applied in the field of preparation of the medicine, can solve the problems of inconspicuous acupuncture effect, inconvenient taking of decoction, slow onset of tablet effect, etc.
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Embodiment 1
[0018] Weigh 1000g each of Sargassum and Honeysuckle, decoct twice with 10 times the amount of water, each time for 1 hour, filter, combine the filtrate, concentrate under reduced pressure to a relative density of 1.21 (50°C), add ethanol to precipitate, and make the alcohol containing reach 65%, refrigerate, take the supernatant, recover the ethanol, and concentrate to a relative density of 1.10 (50°C), let it stand, filter, adjust the pH to 1.5 with dilute hydrochloric acid, extract with 6 times the amount of ethyl acetate, and combine The extract is recovered from ethyl acetate, dried under reduced pressure, and pulverized to obtain a semi-finished product. Take the above semi-finished product, add it to 700ml of water for injection, stir to dissolve, refrigerate, take the supernatant for ultrafiltration, collect the ultrafiltrate, add water for injection to 1000ml, add 0.7% Tween-80 to dissolve, and dissolve with 40% sodium hydroxide Adjust the pH value of the solution to ...
Embodiment 2
[0020] Weigh 1000g of sargassum and 1100g of honeysuckle, decoct twice with 10 times the amount of water, 2 hours each time, filter, combine the filtrate, concentrate under reduced pressure to a relative density of 1.23 (50°C), add ethanol to precipitate, and make the alcoholic reach 70%, refrigerate, take the supernatant, recover the ethanol, concentrate to a relative density of 1.05 (50°C), let stand, filter, adjust the pH to 2.0 with dilute hydrochloric acid, extract with 8 times the amount of ethyl acetate, and combine the extractions liquid, recovered ethyl acetate, dried under reduced pressure, and crushed to obtain a semi-finished product.
[0021] Take the above semi-finished product, add it to 800ml of water for injection, stir to dissolve, refrigerate, take the supernatant for ultrafiltration, collect the ultrafiltrate, add water for injection to 1000ml, add 0.8% Tween-80 to dissolve, and dissolve with 40% sodium hydroxide The pH of the solution was adjusted to 7.0, ...
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