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Pearly lustre pigment coded polymer micro ball and its preparing method

A pearlescent pigment and polymer technology, which is applied to the field of polymer microspheres encoded by pearlescent pigments and the preparation thereof, can solve the problems of high production equipment requirements, uneven particle size and high production cost, and achieves reduction of application cost and preparation. Simple installation and low cost effect

Inactive Publication Date: 2006-09-13
SOUTHEAST UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Commonly used polymer microsphere preparation methods include emulsion polymerization, dispersion polymerization, seed polymerization, suspension polymerization and microsuspension polymerization, etc., but the particle size of microspheres prepared by this method is in the nanometer and submicron range, and will Difficulty encapsulating certain particles in polymers
The methods for preparing polymer microspheres with a particle size of several hundred microns to several millimeters include spray drying method and template method, but there are problems such as uneven particle size, high requirements for production equipment, and high production cost.

Method used

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  • Pearly lustre pigment coded polymer micro ball and its preparing method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Example 1: Preparation of green pearlescent pigment-encoded carboxyl-modified polystyrene microspheres

[0026] ① dissolving the carboxy-modified polystyrene solid in a mixed solvent of ethylene dichloride and benzene, so that the concentration of the carboxyl-modified polystyrene solid in the mixed solvent of ethylene dichloride and benzene is 7%, and dichloroethane and benzene The mixing ratio of benzene is 1:1;

[0027] ②Add green pearlescent pigment to the polystyrene solution at a ratio of 0.5mg pearlescent pigment / ml polymer solution, and stir evenly;

[0028] ③The diameter of the tip of the tip glass tube 4 is set to 200 μm, and the distance between the upper port of the glass conduit 5 and the tip of the tip glass tube is 1 mm;

[0029] ④ Inject 5% polyvinyl alcohol solution into the glass cylinder through the interface 2 of the electromagnetic pump. When the glass cylinder 3 is filled with the polyvinyl alcohol solution, control the injection speed of the poly...

Embodiment 2

[0033]Example 2: Preparation of purple pearlescent pigment-coded polymethyl methacrylate microspheres

[0034] ① Dissolve polymethyl methacrylate in a mixed solvent of ethylene dichloride and benzene, so that the concentration of polymethyl methacrylate in the mixed solvent of ethylene dichloride and benzene is 5%, and ethyl chloride and benzene The mixing ratio is 2:3;

[0035] ②Add green pearlescent pigment to the polystyrene solution at a ratio of 0.7mg pearlescent pigment / ml polymer solution, and stir evenly;

[0036] ③Set the diameter of the tip of the tip glass tube 4 to be 200 μm, and the distance between the upper port of the glass conduit 5 and the tip of the tip glass tube is 1.5 mm;

[0037] ④ Inject 5% polyvinyl alcohol solution into the glass cylinder through the electromagnetic pump interface 2, and when the glass cylinder (3) polyvinyl alcohol solution is filled, control the injection speed of the polyvinyl alcohol solution to 20ml / min;

[0038] ⑤Inject the po...

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Abstract

The present invention relates to pearly luster pigment coded polymer microballoon and its preparation process, and the polymer microballoon is used as the high flux carrier in multiple biological analysis and protein, gene and medicine screening. The polymer microballoon consists of polymer and mica titanium pearlitic pigment, the polymer may be polystyrene, polymethyl methacrylate, polyacrylonitrile, polyethylene, polypropylene or polyethyl acrylate, and the mica titanium pearlitic pigment has the content of 9-80 g / kg. The preparation process includes dissolving polymer in organic solvent to form polymer solution, dropping the polymer into PVA solution and volatilizing organic solvent to obtain the polymer microballoon.

Description

technical field [0001] The invention relates to a polymer microsphere that can be used as a high-throughput carrier for multiple biological analysis and protein, gene, and drug screening, in particular to a polymer microsphere encoded by pearlescent pigments and a preparation method thereof. Background technique [0002] After the human genome sequence was decoded, the function of the gene and the interaction between the proteins encoded by the gene became a research hotspot, and human beings entered the post-genome era. A notable feature of the post-genome era is to study a large number of interactions between proteins and nucleic acids, proteins and proteins, and proteins and drugs. The study of these interactions is almost impossible with traditional experimental methods. Therefore, a high-throughput test platform is needed. The high-throughput test platform requires a high-throughput molecular carrier to identify the different interactions of d...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08J3/12C08L25/06C08L33/12C08L33/20C08L23/12C08L33/08C08K3/34
Inventor 顾忠泽长井圭治赵祥伟杨菡
Owner SOUTHEAST UNIV
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