The invention relates to a preparation method of
titanium dioxide, in particular to a method for preparing high-purity ultra-fine
titanium dioxide by industrial
metatitanic acid. The method includes the steps: a, beating dispersion: washing and bleaching hydrolyzed
metatitanic acid, adding water for
dilution, performing beating and
ultrasonic dispersion to obtain
slurry, adding dispersing agents into the
slurry and performing dispersion to obtain
metatitanic acid slurry; b, curing: curing the metatitanic acid slurry, cooling the metatitanic acid slurry to 60-70 DEG C, and filtering and washing the metatitanic acid slurry until
ferrous ions are removed to obtain a purified metatitanic acid
filter cake; c, calcining: adding water to the metatitanic acid
filter cake, performing
ultrasonic dispersion and calcining, cooling the
filter cake to
room temperature, and crushing and
grinding the filter cake to obtain the
titanium dioxide. By the aid of an
impurity ion occurrence form in hydrolyzed metatitanic acid particles and composition and structural characteristics of the metatitanic acid, the high-purity ultra-fine
titanium dioxide is directly prepared by dispersion, washing, curing, calcining and the like, new varieties of the
titanium dioxide can be increased, product application can be functionalized, and the method has a wide application prospect.