1067 results about "Wet oxidation" patented technology

Methods of performing a wet oxidation process on a silicon containing dielectric material filling within trenches or vias defined within a substrate are provided. In one embodiment, a method of forming a dielectric material on a substrate includes forming a dielectric material on a substrate by a flowable CVD process, curing the dielectric material disposed on the substrate, performing a wet oxidation process on the dielectric material disposed on the substrate, and forming an oxidized dielectric material on the substrate.

The present invention provides a method for manufacturing a semiconductor device having an alignment feature. The method for manufacturing the semiconductor device, among other steps, may include implanting an n-type dopant into a substrate thereby forming an implanted region and an unimplanted region in the substrate. The method may further include oxidizing the substrate using a wet oxidation process, the wet oxidation process and n-type dopant causing a ratio of oxidation of the implanted region to the unimplanted region to be 2:1 or greater, and then removing the oxidized portions of the substrate thereby leaving an alignment feature proximate the implanted region.

The invention is directed to a method and apparatus for treating wastewater. The wastewater treatment system includes a bioreactor including activated carbon and a first biological population. The wastewater treatment system may also include a membrane bioreactor and/or a wet oxidation unit.

A method wherein lignocellulosic biomass materials are converted into combustible fuel products. In particular, the method is a continuous process. involving wet oxidation or steam explosion, for fermentatively converting such biomass materials into ethanol using a process design that permits all or part of the process water from the ethanol fermentation process to be recycled to reduce the consumption of process water. The effluent from the ethanol fermentation step may be subjected to an anaerobic fermentation step generating methane and a water effluent in which the amount of potentially inhibitory substances is at a sub-inhibitory level, which in turn permits all or part of the effluent water from the anaerobic fermentation step to be recycled into the process.

Semiconductor devices, structures and systems that utilize a polysilazane-based silicon oxide layer or fill, and methods of making the oxide layer are disclosed. In one embodiment, a polysilazane solution is deposited on a substrate and processed with ozone in a wet oxidation at low temperature to chemically modify the polysilazane material to a silicon oxide layer.

Disclosed are: a catalyst which can exhibit an excellent catalytic activity and excellent durability for a long period in the wet oxidation treatment of waste water; a wet oxidation treatment method for waste water using the catalyst; and a novel method for treating waste water containing a nitrogenated compound, in which a catalyst to be used has a lower catalytic cost, the waste water containing the nitrogenated compound can be treated at high purification performance, and the high purification performance can be maintained. The catalyst for use in the treatment of waste water comprises an oxide of at least one element selected from the group consisting of iron, titanium, silicon, aluminum, zirconium and cerium as a component (A) and at least one element selected from the group consisting of silver, gold, platinum, palladium, rhodium, ruthenium and iridium as a component (B), wherein at least 70 mass% of the component (B) is present in a region positioned within 1000 [mu]m from the outer surface of the component (A) (i.e., the oxide), the component (B) has an average particle diameter of 0.5 to 20 nm, and the solid acid content in the component (A) (i.e., the oxide) is 0.20 mmol/g or more. The waste water treatment method uses a catalyst (a pre-catalyst) which is placed on an upstream side of the direction of the flow of the waste water and can convert the nitrogenated compound contained in the waste water into ammoniacal nitrogen in the presence of an oxidizing agent at a temperature of not lower than 100 DEG C and lower than 370 DEG C under a pressure at which the waste water can remain in a liquid state and a downstream-side catalyst (a post-catalyst) which is placed downstream of the direction of the flow of the waste water and can treat the waste water containing ammoniacal nitrogen.

The invention discloses a preparation method of a catalytic wet oxidation catalyst and a treatment method of organic wastewater. The preparation method comprises the following steps of: (1) taking a porous inert material as a carrier, and performing pre-impregnation treatment on the carrier by adopting an organic acid solution; and (2) preparing an impregnating solution with a water-soluble compound containing transition metal elements and a water-soluble compound containing auxiliary elements, impregnating the carrier after treatment in the step (1) with the impregnating solution, drying in shade for 12-48 hours in air at appropriate humidity, then drying and roasting to obtain a final catalyst. When the catalyst prepared by the method disclosed by the invention is used for high-concentration organic wastewater, the characteristics of high activity, good stability and the like are realized, and the energy consumption and the investment can be reduced.

The invention discloses a method for treating waste lye by high-temperature wet oxidation. At 220°C to 260°C and under the pressure of keeping the waste lye in liquid phase, the waste lye is contacted with air exceeding the theoretical oxygen demand, and the waste lye is used The oxygen in the air oxidizes the inorganic sulfide and organic matter in the waste caustic so that the sulfur in it is converted into sulfate, and the organic matter is oxidized and decomposed into water and carbon dioxide; the reacted material discharged from the wet liquid phase oxidation reactor enters the high-pressure gas-liquid separator , The oxidized spent lye after gas-liquid separation and the waste lye feed are exchanged for heat, and the oxidized spent lye after heat exchange and the gas phase separated from gas and liquid enter the cooling and washing tower. Compared with the prior art, the method of the present invention has low energy consumption, the removal rate of S2- can reach 100%, the removal rate of COD can reach 75%-85%, and the waste lye after treatment can be directly discharged into the sewage treatment system, effectively alleviating the The pressure brought by the high concentration of wastewater in sewage treatment plants.

The present invention relates to a catalyst for wastewater treatment and a method for wet oxidation treatment of wastewater using the catalyst, in particular, the catalyst of the present invention can suitably be used in wet oxidation treatment of wastewater, under high temperature and high pressure conditions. The present invention provides a catalyst for wastewater treatment containing a catalytic active constituent containing at least one kind of an element selected from the group consisting of manganese, cobalt, nickel, cerium, tungsten, copper, silver, gold, platinum, palladium, rhodium, ruthenium and iridium, or a compound thereof, and a carrier constituent containing at least one kind of an element selected from the group consisting of iron, titanium, silicon, aluminum and zirconium, or a compound thereof, characterized in that solid acid amount of the carrier constituent is equal to or more than 0.20 mmol/g.

A wet oxidation/reduction electrolytic cell stack, system, and method for the remediation of contaminated water is disclosed. A porous electrode of large surface area produces powerful oxidizing agents in situ without having to add any reagents, oxidizers, or catalysts to the water to be treated. Further, by the appropriate selection of electrode material, organic contaminants may be absorbed onto the surface of the electrode and subsequently oxidized to provide a dynamically renewable porous electrode surface. Flow rates, and power requirements may be tailored to the specific moieties to be removed, thus allowing local treatment of specific waste streams resulting in direct discharge to a publicly owned treatment works (POTW) or surface water discharge. A novel feature of this invention is the ability to remove both organic and metal contaminants without the addition of treatment reagents or catalysts.

A process and system for the destruction of compounds having a carbon-hetero atom bond. The process includes wet oxidation at elevated temperature and pressure of an aqueous mixture of at least one compound having a carbon-hetero atom bond to substantially destroy the carbon-hetero atom bond of the at least one compound. The resulting oxidized material may be further treated in an advanced oxidation process to destroy any residual carbon-hetero atom bonds remaining.

The invention relates to a method for preparing iron phosphate from ferrophosphorus. The ferrophosphorus is used as a part or the whole of a phosphorus source and an iron source for preparing the ironphosphate. The phosphorus source or the iron source is supplemented according to a mol ratio of (0.8-1.2):1.0 between total phosphorus elements and total iron elements. The ferrophosphorus is roastedin a dry and oxygen-containing atmosphere. The iron phosphate product is obtained by means of dry or wet oxidation product reaction. The method adopts the ferrophosphorus as the raw material for preparing the iron phosphate, makes full use of elements in the ferrophosphorus and creates a novel preparing process of iron phosphate. In addition, as the reaction process can be used for weakening or eliminating the influence of impurity elements in the ferrophosphorus on the iron phosphate product, the method indirectly purifies the ferrophosphorus and eliminates the influence of the impurities inthe ferrophosphorus and the problem of severe corrosion caused by the existence of water during the roasting of ferrophosphorus. The reaction process has relatively low demand on apparatuses. The preparing method has simple process, short production flow and low production cost, is clean and environment-friendly, realizes high resource utilization rate, low investment and good benefit and is suitable for large-scale, industrial, low-cost and clean preparation of iron phosphate.

The invention discloses a method for rapidly and efficiently degrading pollutants through ultraviolet catalytic wet oxidation at the normal temperature and normal pressure and designs a typical device for implementing the method. In the method, ultraviolet light, an oxidant and a catalyst are introduced into a reaction system; and a wet oxidation reaction can be performed under the mild conditions of normal temperature and normal pressure by utilizing the synergistic catalytic oxidation of the ultraviolet light, the oxidant and the catalyst. Compared with the traditional catalytic wet oxidation method which needs to be implemented under the reaction conditions of high temperature and high pressure, the method can be implemented under the conditions of a temperature of between 25 and 80 DEG C and normal pressure, wherein organic pollutants in high-concentration toxic and hazardous waste water can be decomposed to be harmless components such as carbon dioxide (CO2), water and the like through the high oxidizing property; and the removal rate of chemical oxygen demand (COD) chromium (Cr) after the treatment of a plurality of representative high-concentration organic waste water can reach over 95 percent, and the biochemical property can be improved obviously. The method has the advantages of mild reaction, high treating efficiency, complete degradation, clean and environmental-friendly process, energy conservation and wide application prospect.

The invention discloses a method and a device for treating high-salt refractory organic wastewater, and particularly relates to a method and a device for treating high-concentration refractory COD and high-salt industrial wastewater by coupling the catalytic wet oxidation and MVR evaporation and concentration crystallization technology. The device comprises a vapor-liquid heat exchanger, a liquid-liquid exchanger, a booster pump (or a circulating pump), a compression fan, an oxidant dosing device, a wet catalytic oxidation reactor (WAO), an evaporator, a vapor compressor and a vapor-water separator. Raw water is subjected to air catalytic wet oxidation in the WAO reactor after two-stage preheating through the vapor-liquid heat exchanger and the liquid-liquid exchanger; the oxidized wastewater is evaporated and concentrated by an evaporator to obtain crystalline salt and the distilled water. The method and the device provided by the invention combine advantages of a wet oxidation technology and an MVR technology, effectively degrade organic matters, improve biodegradability of wastewater, and realize effective utilization of heat energy generated by WAO oxidation reaction and secondary vapor of the evaporator.

A wet oxidation/reduction electrolytic cell, system, and method for the remediation of contaminated water is disclosed. A porous electrode of large surface area produces powerful oxidizing agents in situ without having to add any reagents, oxidizers, or catalysts to the water to be treated. Further, by the appropriate selection of electrode material, organic contaminants may be absorbed onto the surface of the electrode and subsequently oxidized to provide a dynamically renewable porous electrode surface. Flow rates, and power requirements may be tailored to the specific moieties to be removed, thus allowing local treatment of specific waste streams resulting in direct discharge to a publicly owned treatment works (POTW) or surface water discharge. A novel feature of this invention is the ability to remove both organic and metal contaminants without the addition of treatment reagents or catalysts.

A process for treating the phenol contained sewage by catalytic wet oxidizing method features that its catalyst is prepared from the active component chosen from Pt, Pd, Rh and Ru, the auxiliary component chosen from La, Ce, Pr and Nd, and TiO2-ZrO2 carrier through baking at 60-180 deg.C for 2-18 hrs and calcining at 300-800 deg.c for 2-18 hrs. It is applied under the conditions: 220-280 deg.C for reaction temp, 4-8 MPa for pressure, 50-300 for air/water ratio, and 0.5-6 /hr for space speed. Its advantages are high reaction efficiency, high removal rate of COD up to 99%, and high BOD5/CODcr increased from 0.02 to 0.6.

The invention relates to an advanced treatment process and device of coal chemical industry wastewater. The process comprises the following steps: removing oil, performing deacidification and deamination, performing centrifugal extraction and dephenolization, performing catalytic wet oxidation and performing biochemical treatment. The device comprises an oil removal pool, a deacidification and deamination regulating reservoir, an ammonia still, a high speed centrifuge, a catalytic wet oxidation regulating reservoir, a catalytic wet oxidation tower, a biochemical regulating reservoir and an A/O biochemical system which are connected with one another sequentially. The indirect emission standard requirements in the national coking chemical industrial pollutant discharge standard (GB16171-2012) can be met after main pollutants such as chemical oxygen demand (COD), oil, ammonia nitrogen and phenol in coal chemical industry wastewater are treated, and ammonia water and crude phenol can be recovered. Compared with the prior art, the advanced treatment process of coal chemical industry wastewater has the beneficial effects that sewage produced in coal chemical industry is treated with a clear target on the basis of characteristics of the coal chemical industry production process, so that the indirect emission standard requirements are met, available resources in the sewage are recovered, and sewage resource treatment is really realized.

The present invention provides a method for treatment of lignocellulosic organic waste or biomass, by which the carbohydrates are rendered more available for subsequent hydrolysis, e.g. by means of addition of enzymes or direct fermentation to one or more desired products. The invention more specifically relates to a method comprising a combination of the following process steps: thermal hydrolysis, wet oxidation and wet explosion. The method according to the present invention can operate with undivided or only poorly divided substrate having a high dry matter concentration.

A catalyst for treating the photoresist sewage by catalytic wet oxidizing process is prepared from the active component chosen from Pt, Pd, Rh and Ru, the auxiliary component chosen from La, Ce, Pr and Nd, and TiO2-ZrO2 carrier through baking at 60-180 deg.c for 2-18 hrs and calcining at 300-800 deg.C for 2-18 hrs. It is applied under the conditions: 220-280 deg.c for reaction temp, 4-8 MPa for reaction pressure, 50-300 for air/sewage ratio and 0.5-6/hr for space speed. Its advantages are high reaction efficiency, high removal rate of COD up to 99%, and high BOD5/CODcr ratio increased from 0.02 to 0.6.

A method for treating desulfurization waste liquid of a wet oxidation method. The method comprises the following steps: firstly adding a decolorant into desulfurization waste liquid for decolorizing treatment, filtering after decolorization, adding alkali into the filtrate, controlling the PH to be 8-9, performing evaporation concentration under a condition with a negative pressure, condensing the evaporated ammonia gas and water vapor to obtain concentrated ammonia liquor which can be returned to the system for recycle or be used to produce ammonium sulfate, performing fractional crystallization of the concentrated desulfurization liquid to respectively obtain high-purity sodium thiocyanate and sodium hyposulfite. The invention has a simple process, and stable operations, and effectively solves the problem of difficult HPF desulfurization waste liquid treatment in coking enterprises; the method not only reduces the discharge of the waste liquid, but also recovers a lot of chemical products with economic value, and the method has quite significant economic benefits and environmental benefits.

A method of manufacture of an avalanche photodiode involving a step of making a recess in a top window layer of an avalanche photodiode layer stack, such that a wall surrounding the recess runs smoothly and gradually from the level of the recess to the level of the window layer. Further, diffusing a dopant over the entire window layer area so as to form a p-n junction at the bottom of the recess, and providing a first electrical isolation region around the recess by buried ion implantation or wet oxidation in order to limit the flow of electrical current to the p-n junction. Forming an isolation trench around the photodiode and a second electrical isolation region by ion implantation into the trench such that the second electrical isolation region runs through the absorption layer of the photodiode.