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Method for detecting constituents of liquorice-ginseng capsule

A technology of Ganshen capsule and detection method, which is applied in the directions of measuring device, material separation, analyzing material, etc.

Active Publication Date: 2006-05-03
SHIJIAZHUANG HUAXIN PHARMA
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  • Abstract
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  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Traditional Chinese patent medicine detection methods can only qualitatively explain the composition of Chinese patent medicine

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Embodiment 1: A method for detecting the component content of finished Ganshen capsules, comprising the following steps and conditions:

[0025] 1. Observation and TLC identification of finished Ganshen capsules

[0026] (1) Observing the finished Ganshen Capsules, the content is brownish yellow to tan powder; the smell is slight and the taste is bitter;

[0027] (2) Take 2 g of the finished product content of Ganshen Capsules, add 40 ml of chloroform, heat and reflux for 1 hour, discard the chloroform solution, evaporate the dregs to remove the solvent, add 0.5 ml of water, stir evenly to moisten, add 10 ml of saturated n-butanol, and process with ultrasonic After 30 minutes, centrifuge, draw the supernatant, add 3 times the amount of n-butanol saturated ammonia test solution, shake well, place layers, take the n-butanol layer, evaporate to dryness, add 1ml of methanol to the residue to dissolve, and use it as the test sample solution.

[0028] Another ginsenoside Re...

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Abstract

The invention relates to a method for measuring Gan Senate capsules. It comprises: identifying the foil of gen-seng, dan-seng and kuh-seng of the Gan Senate capsules and the content of glycyrrhizic acid of Broil licorice roots. It adopts high performance liquid chromatography to measure the content of glycyrrhizic acid of Broil licorice roots and identifies the main elements of gen-seng, dan-seng and kuh-seng of the Gan Senate capsules.

Description

technical field [0001] The invention relates to a component detection method of Ganshen capsules. Background technique [0002] Traditional Chinese patent medicine detection methods can only qualitatively explain the composition of Chinese patent medicines. Efficient and quantitative detection of the components of Chinese patent medicines is an urgent technical problem to be solved in the modern Chinese medicine industry. Contents of the invention [0003] In order to solve the problem of efficiently and quantitatively detecting the component content of Chinese patent medicines, the present invention adopts liquid chromatography technology combined with thin-layer identification technology to provide a method capable of qualitatively and quantitatively testing the component content of Chinese patent medicines. The invention adopts high performance liquid chromatography to detect the content of glycyrrhizic acid in Radix Glycyrrhizae Radix Glycyrrhizae of Ganshen Capsules,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N21/27G01N30/06
Inventor 刘志强李惠琳刘淑莹宋凤瑞金东明
Owner SHIJIAZHUANG HUAXIN PHARMA