Sintered valve guide and manufacturing method thereof
A technology of valve guide and sintered alloy, which is applied in the field of sintered valve guide
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Embodiment 1
[0063] Sample 1~27
[0064] With ore reduced iron powder (containing metal oxide 0.1 mass %) or atomized iron powder (containing metal oxide 0.2 mass %) as raw material iron powder, according to the mixing ratio described in table 1, raw material iron powder and iron-phosphorus Alloy powder, copper-tin alloy powder and graphite powder were mixed to prepare powder mixtures of samples 1-27, respectively. The overall composition of each powder blend sample is shown in Table 2. The particle sizes of various powders are as follows: Mineral reduced iron powder (greater than or equal to 150 μm: 5%, 45-150 μm: 75%, less than 45 μm: 20%), atomized iron powder (greater than or equal to 150 μm: 17%, 45-150 μm: 58%, less than 45 μm: 25%), iron-phosphorus alloy powder (greater than or equal to 63 μm: 3%, 45-63 μm: 10%, less than 45 μm: 87%), copper-tin alloy powder (greater than or equal to 150 μm : 7%, 45-150μm: 73%, less than 45μm: 20%), graphite powder (average particle size: 0.6-0.8m...
Embodiment 2
[0092] Sample 28~38
[0093] Using a powder mixture of the same composition as Sample 4 of Example 1, sintered body samples 28 to 31 were prepared by operations similar to that of Sample 4 (preparation of powder mixture, production of shaped body blanks, sintering and cooling), with the sintering temperature changed , as shown in Table 4, are 900°C (sample 28), 950°C (sample 29), 1050°C (sample 30), and 1100°C (sample 31), respectively. The overall composition of the powder mixture for each sample is shown in Table 5.
[0094] Also, sintered samples 32 to 36 were prepared by operations similar to sample 4 (preparation of mixture powder, manufacture of molded body blanks, sintering and cooling), but the sintering time was changed to 10 minutes (sample 32), 20 minutes (sample 33 ), 45 minutes (sample 34), 90 minutes (sample 35) and 120 minutes (sample 36).
[0095] In addition, sintered body samples 37 and 38 were prepared by operations similar to sample 4 (preparation of mixt...
Embodiment 3
[0115] Sample 39~49
[0116] Sintered body samples 39-42 were prepared from the powder mixtures of the samples listed in Table 7 according to the similar steps of sample 4 (preparation of powder mixture, manufacture of shaped body blanks, sintering and cooling), but contained oxides in the raw iron powder, respectively 0.2% by mass (scale reduced iron powder, sample 39), 0.5% by mass (sample 40), 1.5% by mass (sample 41), and 2.0% by mass (sample 42). The overall composition of the powder mixture for each sample is shown in Table 8.
[0117] Samples 43 to 49 were separately prepared, and the operation was basically the same as that of sample 4 (preparation of powder mixture, manufacture of shaped body blanks, sintering and cooling), except that part or all of the mineral reduced iron powder was atomized iron powder (oxide content: 0.2% by mass ), and its proportion to the total powder mixture is 5 mass % (sample 43), 10 mass % (sample 44), 15 mass % (sample 45), 20 mass % (sa...
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