Tobacco pyrolytic cracking analytical method
An analysis method and pyrolysis technology, which is applied in the field of analysis of pyrolysis release products of tobacco and its products, and can solve problems such as differences in substance release
Active Publication Date: 2011-04-06
CHINA TOBACCO GUANGDONG IND
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- Summary
- Abstract
- Description
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AI Technical Summary
Problems solved by technology
[0005] Problems and deficiencies in existing methods: cracking tobacco samples at instantaneous high temperature ignores that during the smoking process of cigarettes, not only combustion and high temperature cracking exist, but high temperature cracking mainly occurs in the cigarette combustion cone and its surrounding areas, and there are also chemical processes such as distillation and dry distillation. reaction
That is to say, there is a significant difference in the release of substances by simulating the combustion of cigarettes with the existing pyrolysis method
Method used
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Experimental program
Comparison scheme
Effect test
Embodiment 1
[0021] 1. Main instruments and materials
[0022] GC6890N / 5975B Gas Chromatograph / Mass Spectrometer from Agilent, USA; 5200 Thermal Cracker from CDS.
[0023] Tobacco sample: A famous domestic cigarette product, crushed and passed through an 80-mesh sieve.
[0024] 2. Method
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Abstract
Disclosed is an analysis method for tobacco thermal cracking, simulating the burning state during the cigarette smoking with different temperature areas set for low-temperature thermal purging of samples before a high-temperature cracking, and then products being introduced into a test equipment for qualitative and quantitative analysis. The invention realizes a complete simulation of the cigarette smoking process by the thermal cracking equipment, more close to the substance release state in the cigarette smoking process, facilitating a follow-up accurate detection and analysis of the tobacco and the combustion product thereof.
Description
technical field [0001] The invention belongs to the technical field of analysis and detection, and in particular relates to an analysis method for pyrolysis release products of tobacco and its products. Background technique [0002] There is a certain relationship between the chemical composition of cigarette shredded tobacco and cigarette smoke. The composition of smoke is formed by complex processes such as combustion, cracking, degradation, and distillation of shredded tobacco, among which cracking is a very important link. [0003] The pyrolysis process of cigarettes is very complicated, it is difficult to control its combustion temperature and combustion environment, and it is difficult to study and analyze. For this reason, some scholars use a pyrolyzer to crack tobacco samples, which can simulate the process of burning cigarettes. This method can easily control the conditions of cigarette thermal cracking, such as temperature, environment, etc., and because the crack...
Claims
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Patent Type & Authority Patents(China)
IPC IPC(8): G01N1/44
Inventor 孔浩辉
Owner CHINA TOBACCO GUANGDONG IND
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