Shearing cross-linking sensitive plugging agent and preparation method thereof
A technology of sensitivity and plugging agent, which is applied in the field of shear cross-linking sensitive plugging agent and its preparation, and can solve the problems of affecting drilling efficiency, affecting drilling speed, repetitive leakage, etc.
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[0018] Below by embodiment the present invention will be further described:
[0019] (1) Preparation of organic titanium kerosene solution
[0020] As a cross-linking agent, organic titanium can link polymer chains containing ~OH to form a body structure. Organic titanium is a titanate compound such as: tetraisopropyl orthotitanate, diisopropyl orthotitanate dilactic acid Any one of ester, bis-triethanolamine diisopropyl orthotitanate, mix organic titanium with kerosene to form organic titanium kerosene solution, the concentration (mass percentage) of organic titanium crosslinking agent in kerosene is 0.1~1.0% .
[0021] (2) preparation of modified guar gum aqueous solution
[0022] Modified guar gum is used as a thickening agent, which is obtained by graft copolymerization of acrylamide, methylolacrylamide monomer and guar gum. The graft copolymerization process is: 0.5-1.5 parts of guar gum Disperse and dissolve, pass nitrogen gas for 1 hour, add 0.001~0.01 parts of ammon...
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