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Lindera reflexa Hemsl ethylacetate part extract and application thereof

A technology of ethyl acetate and ethyl acetate of sycamore is applied in the field of medicine and achieves the effects of stable quality and simple preparation method

Active Publication Date: 2012-02-29
HENAN UNIV OF CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In view of the above situation, the object of the present invention is to provide an extract of ethyl acetate part of the mountain peony and its application, that is, an effective part substance extracted from the root of the mountain peony with ethyl acetate, which can be used in the preparation, treatment and prevention of deficiency cold in the spleen and stomach. The application in chronic gastritis and gastric ulcer drugs can effectively solve the problem of preparing and preventing chronic gastritis and gastric ulcer drugs

Method used

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  • Lindera reflexa Hemsl ethylacetate part extract and application thereof
  • Lindera reflexa Hemsl ethylacetate part extract and application thereof
  • Lindera reflexa Hemsl ethylacetate part extract and application thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0012] Take the root of the root, crush it, pass through a 24-mesh sieve, take the root powder and extract it with petroleum ether with a boiling point of 60-90°C for 3 times, add 6 times the weight and volume of the root powder for the first and second times Reflux extraction of petroleum ether for 2 hours, reflux extraction of 2 hours by adding 4 times the weight and volume of the root powder of the root powder for the third time, suction filtration, discarding the filtrate, and then carrying out reflux extraction with ethyl acetate for 3 times, the first time , the second time all add the ethyl acetate of 6 times of the weight and volume of the root powder of the mountain root to reflux for 2 hours, add the ethyl acetate of the weight and volume of the root of the root of the 4 times the amount for the third time and reflux for 2 hours, suction filter, vacuum decompression The ethyl acetate was recovered, concentrated and dried at 45°C to obtain a dry powder, namely the extr...

Embodiment 2

[0014] Take the root of the root, crush it, pass through a 24-mesh sieve, take the root powder and extract it with petroleum ether with a boiling point of 60-90°C for 3 times, add 8 times the weight and volume of the root powder for the first and second times Reflux extraction of petroleum ether for 3 hours, adding 6 times the amount of petroleum ether of the root powder weight volume for the third time for reflux extraction for 3 hours, suction filtration, discarding the filtrate, and then carrying out reflux extraction with ethyl acetate for 3 times, the first time , the second time all add the ethyl acetate of 8 times of the weight and volume of the root powder of the root of the mountain to reflux for 3 hours, add the ethyl acetate of the weight and volume of the root of the root of the 6 times of the amount of the root of the root of the root of the reflux for 3 hours for the third time, suction filter, vacuum decompression The ethyl acetate was recovered, concentrated and...

Embodiment 3

[0016] Take the root of the root, crush it, pass through a 24-mesh sieve, take the root powder and extract it with petroleum ether with a boiling point of 60-90°C for 3 times, add 10 times the weight and volume of the root powder for the first and second times Reflux extraction of petroleum ether for 4 hours, reflux extraction of petroleum ether with 8 times the weight and volume of the root powder of the root powder was added for the third time for 3 hours, suction filtration, discarding the filtrate, and then carrying out reflux extraction with ethyl acetate for 3 times, the first time , the second time all add 10 times the amount of Ethyl Acetate of the weight and volume of the root powder of the root of the mountain to reflux for 4 hours; The ethyl acetate was recovered, concentrated and dried at 60°C to obtain a dry powder, namely the extract of the ethyl acetate part of the mountain beetle.

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Abstract

The invention relates to a Lindera reflexa Hemsl ethylacetate part extract and an application thereof, which can effectively solve the problem of preparing drugs for curing and preventing chronic gastritis and gastric ulcer. The extract is prepared by the following steps: taking Lindera reflexa Hemsl root, crushing, sieving, refluxing and extracting Lindera reflexa Hemsl root powder for three times by petroleumether with a boiling point of 60-90 DEG, pumping and filtering, abandoning filtrate, refluxing and extracting for three times by ethylacetate, pumping and filtering, decompressing in vacuum and recovering ethylacetate, concentrating and drying at the temperature of 40-60 DEG C to obtain dry powder with the yield of 2.48%. The preparation method of the invention is simple and convenient, and the obtained effective part extract has stable quality, can be effectively used for preparing drugs for curing and preventing spleen-stomach deficiency-cold chronic gastritis and gastric ulcer, opens up a novel field for Lindera reflexa Hemsl to prepare drugs and is an innovation in traditional Chinese medicine and pharmacology.

Description

1. Technical field [0001] The invention relates to the field of medicine, in particular to an extract from the part of ethyl acetate of arborescens and its application. 2. Background technology [0002] Lindera reflexa Hemsl. is a plant of the genus Piper in the family Lauraceae, which is a shrub or small tree. It is mainly distributed in the Dabie Mountains, Tongbai Mountains, Jiangsu, Anhui and other places in Henan. The Xinyang area in Henan is the most widely distributed and has a rich output. The root or bark of the root is used as medicine, warm in nature, pungent in taste, has the effects of promoting qi and relieving pain, strengthening the spleen and eliminating accumulation, promoting blood circulation and reducing swelling. Shanxi has received good results in long-term clinical application, and has a long history of application. Due to its good clinical curative effect and rich medicinal material resources in our province, it was included in the "Standards of Tr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/54A61P1/04A61K125/00
Inventor 陈随清张峰张涛
Owner HENAN UNIV OF CHINESE MEDICINE
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