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Solid fluffing tablet and preparation method thereof

A flake and solid technology, applied in the textile field, can solve the problems of unstable product quality, poor fluffing effect, high cost, etc., and achieve the effect of overcoming the difficulty of lubricating and grasping, good cost conversion, and reduced friction

Active Publication Date: 2013-03-13
YONGCHUN XIANGYI CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Except for a small amount of raw materials, most of the existing fluffing agents in the market are water, which has the disadvantages of transportation and packaging costs, unstable product quality, high cost, and poor fluffing effect

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] (1) Preparation of silicon emulsion smoothing agent

[0035] 201: 50g isomeric tridecanol: 10g water: 60g

[0036] Stir at a high speed of 2800 rpm to emulsify fully and evenly, add 10g of hydrophilic silicone oil, and discharge;

[0037] (2) Synthetic film

[0038] Stearic acid: 45g Triethanolamine: 10g Paraffin: 90g

[0039] React at a high temperature of 160-180°C for 2-4 hours, lower the temperature at 100°C, add 10g of paraffin emulsifier and keep it warm at 100°C for 20 minutes, add (1) all the silicon emulsion smoothing agent, vacuumize at 115-150°C for 2 hours, and cool down Slice at 80°C.

Embodiment 2

[0041] (1) Preparation of silicon emulsion smoothing agent

[0042] Process:

[0043] 201: 50g isomeric tridecanol: 10g water: 60g

[0044] Stir at a high speed of 3000 rpm to emulsify fully and evenly, add 10g of hydrophilic silicone oil, and discharge;

[0045] (2) Synthetic film

[0046] Stearic acid: 45g Triethanolamine: 15g Paraffin: 90g

[0047] React at a high temperature of 160-180°C for 3 hours, cool down at 100°C, add 10g of paraffin emulsifier and 5g of 638 thickener, keep warm at 100°C for 30 minutes, add (1) all the silicon emulsion smoothing agent, and vacuumize at 130°C for 3 Hours, cool down to 80°C and slice.

Embodiment 3

[0049] raw material:

[0050] 201: 40 grams

[0051] Isotridecanol 7g

[0052] Water: 50 grams

[0053] Hydrophilic silicone oil: 7 grams

[0054] Stearic acid: 40 grams

[0055] Triethanolamine: 5 grams

[0056] Paraffin: 70 grams

[0057] Paraffin emulsifier: 5 g.

[0058] Process steps:

[0059] (1) Emulsify 201, isotridecanol and water fully and evenly under high-speed stirring, add silicone oil, and discharge;

[0060] (2) Mix stearic acid and triethanolamine, react at a high temperature of 160-180°C for 2 hours, cool down to 90°C, add paraffin emulsifier, and keep warm at 90°C for 30 minutes;

[0061] (3) Add all the materials obtained in (1) to (2), vacuumize at 100°C for 4 hours, cool down to 75°C and slice into pieces.

[0062] The speed of high-speed stirring described in step (1) is 2000 rpm.

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PUM

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Abstract

The invention belongs to textile technology and provides a novel solid fluffing tablet, which is prepared from the following raw materials in part by weight: 40 to 60 parts of 201, 7 to 15 parts of iso-tridecanol, 50 to 70 parts of water, 7 to 15 parts of silicon oil, 40 to 50 parts of stearic acid, 5 to 25 parts of triethanolamine or diethylenetriamine, 70 to 110 parts of paraffin and 5 to 20 parts of paraffin emulsifier. The solid fluffing tablet can be diluted into 10 percent strong liquor, and also can be directly put into a dipping machine. The solid fluffing tablet is convenient to store and transport, does not waste lots of water and packing materials, and is favorable for environmental protection, low carbon and emission reduction. Silicon and paraffin are introduced into the solid fluffing tablet and have the effects of smoothing and reducing friction, so the solid fluffing tablet facilitates fluffing, can achieve good effect, lower conversion cost and better functional effect, and has more advantages than similar products abroad and at home.

Description

technical field [0001] The invention relates to the field of textiles, in particular to a solid napping sheet for napping of cloth and a preparation method thereof. Background technique [0002] Most of the existing fluffing agents in the market are water except a small amount of raw materials, which has the disadvantages of transportation, packaging costs, unstable product quality, high cost, and poor fluffing effect. Contents of the invention [0003] The invention provides a novel solid fluffing sheet, which is made from raw materials comprising the following proportioning substances in parts by weight: [0004] 201: 40-60 servings [0005] Isomerized tridecanol: 7 to 15 parts [0006] Water: 50-70 parts [0007] Silicone oil: 7 to 15 parts [0008] Stearic acid: 40-50 parts [0009] Triethanolamine: 5-25 parts [0010] Paraffin: 70-110 parts [0011] Paraffin emulsifier: 5-20 parts. [0012] More preferably, it is prepared from raw materials comprising the foll...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L91/06C08L83/04C08K5/09C08K5/17
Inventor 叶天降
Owner YONGCHUN XIANGYI CHEM TECH
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