Composition containing nitrogenous heterocyclic compounds
A compound and composition technology, applied in the field of organic electroluminescent elements, can solve the problem that the brightness half-life of organic electroluminescent elements may not be long, etc.
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[0158] For the composition of the present invention, from the viewpoint of the brightness half-life life of the organic electroluminescent element, it is preferably: a composition containing the compound represented by the above formula (1) and a compound represented by the above formula (2); The composition of the compound of the residue of the compound represented by the above-mentioned formula (1) and the compound represented by the above-mentioned formula (2) or the compound having the residue of the compound represented by the above-mentioned formula (2), and has the above-mentioned formula (1 ) The compound represented by the residue of the compound represented by the above formula (1) is a composition of a polymer compound having a repeating unit comprising the residue of the compound represented by the above formula (1); containing the compound represented by the above formula (1) or having the above formula (1) A compound having a residue of the compound represented by...
Embodiment
[0238] The present invention will be specifically described using examples.
Synthetic example 1
[0239] (Synthesis of Low Molecular Compound A)
[0240]
[0241] Under a nitrogen atmosphere, 100 g (0.65 mol) of trifluoromethanesulfonic acid was added, followed by stirring at room temperature. A solution obtained by dissolving 61.93 g (0.33 mol) of 4-bromobenzonitrile in 851 ml of dehydrated chloroform was added dropwise to the obtained reaction liquid. The obtained solution was heated up to 95° C., stirred while heating, then cooled to room temperature, and dilute ammonia solution was added thereto under an ice-water bath. The obtained solid was removed by filtration, washed with water and then with diethyl ether, and dried under reduced pressure to obtain 47.8 g of white crystals.
[0242]
[0243] Under a nitrogen atmosphere, 8.06 g (14.65 mmol) of white crystals obtained, 9.15 g (49.84 mmol) of 4-tert-butylphenylboronic acid, Pd (PPh 3 ) 4 1.54 g (1.32 mmol), 500 ml of toluene previously bubbled with nitrogen, and 47.3 ml of ethanol previously bubbled with ni...
PUM
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