The invention relates to a high-purity
antimony producing method by a two-section fused salt
electrolysis method. The high-purity
antimony producing method includes: a step of adding smashed
antimony blocks and a fused salt
electrolyte into an
electrolytic cell comprising a first
graphite electrode and a second
graphite electrode; a step of electrolyzing firstly by an
anode method, wherein the first
electrode is set as an
anode, the second electrode is set as a
cathode, in an
anode region, the antimony and
impurity metals lose electrons, become positive ions, enter the fused salts, migrate to the surface of the
cathode under actions of an
electric field and
diffusion and receive the electrons, and the
impurity metals, which have standard electrode potentials lower than the
standard electrode potential of the antimony, comprising Na, K, Zn, Cd, Fe, Pb, Sn, Cu and Ni are removed; and a step electrolyzing firstly by a
cathode method, wherein the first electrode is set as a cathode, the second electrode is set as an anode, the reduced antimony elementary substance is adopted as a cathode, and
nonmetal impurity elements comprising As, S and Bi are removed. The high-purity antimony producing method adopts the two-section fused salt
electrolysis method, and optimizes
electrolysis parameters to obtain antimony having purity of 99.99%. The high-purity antimony producing method is simple in process and suitable for large-scale industrial production.