Methods for identifying fragile histidine triad (Fhit) interaction and uses thereof
A triplet, histidine technology, applied in the fields of botanical equipment and methods, biochemical equipment and methods, applications, etc., can solve problems such as Fhit's little knowledge
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Embodiment I
[0111] Materials and methods
[0112] Cells, Vectors and Antisera - A549, H1299, MKN74-E4 and A116 and HCT116 cells were maintained in RPMI 1640 medium plus 10% fetal bovine serum and penicillin / streptomycin (Sigma). HEK293 cells (Microbix) used to prepare recombinant adenoviruses were cultured in Dulbecco's modified Eagle's medium plus 10% fetal calf serum and penicillin / streptomycin. AdFHIT-His6 virus was prepared as described in Example II herein. [His6-SEQ ID NO: 32] [penta-His-SEQ ID NO: 33].
[0113] Full-length FDXR was cloned from human brain cDNA (Clontech), subcloned into the pcDNA3.1 / V5-HisTOPO TA vector (Invitrogen) and sequenced; details are described in the accompanying methods below. Using Lipofectamine TM (Invitrogen) cells were transfected according to the manufacturer's instructions.
[0114] Western blot analysis - Western blot analysis was performed as described in (13) using: monoclonal anti-pentaHis (Qiagen); rabbit polyclonal anti-Fhit (Zymed Laborat...
Embodiment III
[0124] Production of Recombinant Adenovirus - Recombinant adenovirus carrying wild-type FHIT cDNA (AdFHIT) was prepared as previously described (Ishii et al., 2001 Cancer Res 61: 1578-1584). His-tagged FHIT cDNA was generated by PCR using the following oligonucleotides: 5'-ACgTggATCCCTgTgAggACATgTCgTTCAgATTTggC-3' (forward) [SEQ ID NO: 26] and 5'-TTgTggATCCTTATCAgTgATggTgATggTgATgCgATCCTCTCTgAAAgTAgCCCgCAg-3' [SHQ ID NO: 27]. These primers were designed with a BamHI restriction site for subcloning into the transfer vector pAdenoVator-CMV5-IRES-GFP. Ad-His 6 is using AdenoVator TM Kits (Qbiogene, Carlsbad, CA) were produced according to the manufacturer's protocol. Ad GFP used as a control was purchased from Qbiogene (Carlsbad, CA).
[0125] Generation of recombinant expression vector carrying FDXR cDNA - full-length wild-type ferredoxin reductase was amplified from human brain cDNA (Clontech, Palo Alto, CA) using the following primers: 5'-CTgTTCCCAgCCATggCTTCgCgCTg-3' (forwa...
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