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Additive used for fireworks medicament pelletizing process and adding method thereof

A technology of pyrotechnic agents and additives, applied in non-explosive/non-thermal agent components, explosives, offensive equipment, etc., can solve the problems affecting the physical and chemical properties of pyrotechnic agents, changing the oxygen balance value of the original agent, combustion and explosion, etc., to avoid burning Explosion accidents, low cost, and less dosage

Inactive Publication Date: 2012-10-10
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But at the same time, pyrotechnic agents contain flammable and explosive substances such as aluminum powder and aluminum-magnesium alloy powder. Especially in the granulation process, they will chemically react with binder solvents such as water or alcohol to release heat, resulting in pyrotechnic agent The increase in temperature and the consumption of aluminum powder and magnesium-aluminum alloy powder produce macroscopically perceptible heat and chemical phenomena, that is, the formation of chemical energy, that is, heat generation. When the heat released by the chemical reaction gradually exceeds the heat emitted by the pyrotechnic agent, The heat will be accumulated slowly, and then the temperature will gradually rise, the chemical reaction will accelerate sharply, and the temperature will also rise sharply, so that it will reach the spontaneous ignition point of the agent at a certain moment, causing a combustion explosion accident
Moreover, some binders participate in the reaction of the agent, which changes the oxygen balance value of the original agent and seriously affects the physical and chemical properties of the pyrotechnic agent.

Method used

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  • Additive used for fireworks medicament pelletizing process and adding method thereof
  • Additive used for fireworks medicament pelletizing process and adding method thereof
  • Additive used for fireworks medicament pelletizing process and adding method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] The pyrotechnic formulation used is:

[0014]

[0015] (1) Weigh 41.5g, 8.45g, 19.7g, 9.15g, 21.1g and 1g of sulfur powder, aluminum powder, magnesium-aluminum alloy powder, potassium nitrate, barium nitrate and potassium dichromate respectively and mix them evenly, and weigh Take 2 g of cooked glutinous rice flour to prepare an aqueous solution with a mass fraction of 5%.

[0016] (2) Bonding the mixed medicine obtained in step (1) and the cooked glutinous rice flour aqueous solution into a granular medicine product.

[0017] Place the finished granular medicine directly in a 300ml beaker and seal it with a plastic film. Insert a thermometer into the middle of the beaker and place the beaker at a certain distance from the observation point. At the same time, use another thermometer to measure the ambient temperature. Observe the thermometer reading every ten minutes.

[0018] After adding the additive of the present invention, the temperature of the medicine is kept consisten...

Embodiment 2

[0020] The pyrotechnic formulation used is:

[0021]

[0022] (1) Weigh 41.5g, 8.45g, 19.7g, 9.15g, 21.1g and 2g of sulfur powder, aluminum powder, magnesium-aluminum alloy powder, potassium nitrate, barium nitrate and potassium dichromate respectively and mix them evenly, and weigh Take 3g of cooked glutinous rice flour and mix it with water to form a solution with a mass fraction of 5%.

[0023] (2) Bonding the mixed medicine obtained in step (1) and the cooked glutinous rice flour aqueous solution into a granular medicine product.

[0024] Place the finished granular medicine directly in a 300ml beaker and seal it with a plastic film. Insert a thermometer into the middle of the beaker of medicine, and place the beaker at a certain distance from the observation point. At the same time, use another thermometer to measure the ambient temperature. Observe the thermometer reading every ten minutes.

[0025] After adding the additive of the present invention, the temperature of the medi...

Embodiment 3

[0027] The pyrotechnic formulation used is:

[0028]

[0029]

[0030] (1) Weigh 41.5g, 8.45g, 19.7g, 9.15g, 21.1g and 2g of sulfur powder, aluminum powder, magnesium-aluminum alloy powder, potassium perchlorate, barium nitrate and potassium dichromate respectively and mix them evenly. Take 3g of cooked glutinous rice flour and mix it with water to form a solution with a mass fraction of 5%.

[0031] (2) Bonding the mixed medicine obtained in step (1) and the cooked glutinous rice flour aqueous solution into a granular medicine product.

[0032] Place the finished granular medicine directly in a 300ml beaker and seal it with a plastic film. Insert a thermometer into the middle of the beaker of medicine, and place the beaker at a certain distance from the observation point. At the same time, use another thermometer to measure the ambient temperature. Observe the thermometer reading every ten minutes.

[0033] After adding the additive of the present invention, the temperature of the m...

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Abstract

The invention relates to an additive used for fireworks medicament pelletizing process and an adding method thereof, belonging to the field of fireworks and firecrackers. Potassium dichromate and cooked glutinous rice flour are taken as the additive, wherein the mass of the potassium dichromate accounts for 1%-3% of the total mass of fireworks medicament, and the particle size of the potassium dichromate is smaller than 80 meshes; and the cooked glutinous rice flour is taken as adhesion agent, and the mass of the cooked glutinous rice flour accounts for 1%-4% of the total mass of the fireworks medicament. The adding method is as follows: when mixing medicament raw material, adding potassium dichromate with the mass accounting for 1%-3% of the total mass of the medicament, and the particlesize being smaller than 80 meshes, mixing uniformly; and in the bonding process, replacing the additive by the cooked glutinous rice flour accounting for 1%-4% of the total mass of the medicament, and preparing the cooked glutinous rice flour into 3%-8% of water solution. In the invention, the additive is low in cost, the using amount is little, the adding process is simple, the problem of heat accumulation in the pelletizing process of the fireworks medicament is solved, so that the temperature of the medicament is the same as that of the environment, the explosion accident is avoided, and the additive can not affect the setting-off performance of the original medicament formula.

Description

Technical field [0001] The invention relates to an additive used in a pyrotechnic agent granulation process and an adding method thereof, belonging to the field of fireworks and firecrackers. Background technique [0002] In the production process of pyrotechnics and pyrotechnics, in order to improve the dispersion of the medicament, reduce the dust in the process of screening and charging the medicament, and realize the accurate filling of the medicament, the medicament needs to be granulated. With the development of science, the chemical deposition method, water suspension method, electromagnetic sputtering deposition method and high-speed dispersion agent method have been researched and developed. The pyrotechnic drug granulation process generally first mixes the drug raw materials uniformly, and then uses a binder to bond the raw materials into particles. But at the same time, the pyrotechnic composition contains aluminum powder, aluminum-magnesium alloy powder and other fla...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C06B33/14C06B23/00
Inventor 黄平刘海营钱新明刘振翼
Owner BEIJING INSTITUTE OF TECHNOLOGYGY