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Real time monitoring method for resin rheological property under action of ultrasound, and apparatus thereof

A rheological performance and real-time monitoring technology, applied in the direction of measuring devices, flow characteristics, instruments, etc., can solve the problems of test data errors, changes, and affecting the rheological properties of resins, so as to avoid errors, achieve consistency, and realize real-time testing Effect

Active Publication Date: 2011-11-16
TIANJIN POLYTECHNIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This test method mainly has the following problems: (1) the test environment of the subsection or separate test is not synchronized with the ultrasonic action environment, and there are errors between the test data and the real data; (2) the subsection test is non-real-time monitoring, due to There is a phenomenon of energy attenuation in the propagation of ultrasonic waves, and the difference in the ultrasonic sound pressure gradient in the effective space of the ultrasonic wave directly affects the change of the rheological properties of the resin.
[0009] From the above analysis, it can be seen that the existing detection methods and devices cannot accurately and real-time reflect the change law of the rheological properties of the resin under the action of ultrasound.
Within the scope of the applicant's search, there are no reports on the real-time monitoring device and method for the change of resin rheological properties under the action of ultrasound.

Method used

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  • Real time monitoring method for resin rheological property under action of ultrasound, and apparatus thereof
  • Real time monitoring method for resin rheological property under action of ultrasound, and apparatus thereof
  • Real time monitoring method for resin rheological property under action of ultrasound, and apparatus thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0033] This embodiment adopts the monitoring device of the present invention (see figure 1 ), real-time testing of resin rheological properties while ultrasonically treating the resin. Its parameters are as follows:

[0034] The output power of the ultrasonic generator 42 is respectively 1200W, 1400W and 1600W; the vibration frequency of the ultrasonic transducer 41 is 20KHz; the ultrasonic amplitude is respectively 23 μm, 28 μm and 33 μm; The program is adjusted to achieve constant temperature measurement at 28°C; the resin used in the experiment is: JL-237 epoxy resin produced by Changshu Jiafa Chemical Co., Ltd. The specific test method is as follows:

[0035] (1) Preparation work before the test, put the resin to be tested into the resin container 3, connect the ultrasonic device and the viscosity tester 11, and zero-adjust the viscosity tester 11; (2) temperature control, open the oil bath The power supply heats the resin in the resin container 3, and through the adju...

Embodiment 2

[0038] The resin used in the experiment of this embodiment is 86# epoxy resin, and the test temperature of the resin is 50° C., and the remainder is the same as in Example 1.

[0039] The test results are as follows: when the ultrasonic amplitude is 23um, the resin in the resin container has circulation around the horn, and some cavitation bubbles can be observed to form and collapse, and the viscosity of the untreated resin is reduced by about 43%; when the ultrasonic amplitude is 28um , the resin in the resin container has obvious circulation around the horn, and the generation and collapse of many cavitation bubbles can be observed, and the viscosity of the untreated resin is reduced by about 39%; when the ultrasonic amplitude is 33um, the resin in the resin container becomes The rod has obvious circulation phenomenon, and the generation and collapse of a large number of cavitation bubbles can be observed, and the viscosity of the untreated resin is reduced by about 48%.

Embodiment 3

[0041] This embodiment adopts the monitoring device of the present invention (see figure 1 ), real-time monitoring of the rheological properties of the resin while ultrasonically treating the resin, its parameters are as follows:

[0042] The output power of the ultrasonic power supply 42 is 1400W; the vibration frequency of the ultrasonic transducer 41 is 20KHz; Constant temperature measurement under different temperature conditions; the resin used in the experiment is 86# epoxy resin. The specific test method is as follows:

[0043] (1)-(2) are the same as embodiment 1. (3) The test of viscosity, by observing the resin temperature displayed in real time by the temperature tester, when the resin temperature reaches 28°C, open the ultrasonic generator 42 and start to perform ultrasonic action on the resin and adjust its output power to be 1400W (at this time, ultrasonic The amplitude is 28 μm), and at the same time, the control program of the viscosity tester is turned on ...

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Abstract

The invention discloses a real time monitoring method for resin rheological property under an action of ultrasound, and an apparatus thereof. The monitoring method is characterized by: directly putting a detection sensor in a resin container under the action of the ultrasound; carrying out dynamic, real-time, multi-point and exact measuring and monitoring for resin viscosity and the resin rheological property when the resin is under the action of the supersonic vibration. The apparatus comprises a viscosity tester, a temperature controller, a bathtub, a temperature tester and the resin container. The apparatus is characterized in that: the apparatus further comprises an ultrasonic transducer, a ultrasonic generator, a fixing apparatus and a isolation apparatus, wherein the ultrasonic transducer is arranged in the isolation apparatus through the fixing apparatus, a tool rod of the ultrasonic transducer sequentially passes through the isolation apparatus and a side wall of the resin container, and enters into the resin container, and is provided for directly acting on the resin requiring detection. The tool rod can be freely adjusted in three dimensions, wherein the tool rod can swing up and down, left and right, and stretch forward and backward in the resin container, such that real time measuring and monitoring of the resin rheological property at different space position points on the face under the action of the ultrasound are realized.

Description

technical field [0001] The invention relates to resin rheological performance monitoring technology, in particular to a real-time monitoring method and device for resin rheological performance under ultrasonic action. Background technique [0002] With its cavitation effect, acoustic flow effect and thermodynamic effect, high-energy ultrasound can promote the formation and collapse of cavitation bubbles in liquids, enhance the flow of liquids, and reduce the viscosity of liquids. modified. In recent years, there are more and more applications of ultrasonic action to improve the rheological properties of resins, such as the ultrasonic treatment resin transfer molding method and its devices reported in Chinese patent 03132430.4, which improves the infiltration of resin to fibers during RTM molding properties, which reduces the void content, thereby improving the interfacial properties of the composite material; another example is Chinese patent 202010126838.7, which reports a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N11/00
Inventor 张国利王富有陈利陈光伟李嘉禄
Owner TIANJIN POLYTECHNIC UNIV
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