Method for preparing feeding nozzle for continuous high-purity alumina melting furnace and continuous melting furnace
A technology of high-purity alumina and melting furnaces, which is applied in the direction of furnaces, crucible furnaces, furnace types, etc., can solve the problems of inner tank materials that cannot meet the requirements of use, and achieve high overall reliability, maintain no pollution, and uniform microstructure Effect
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Embodiment 1
[0015] Mix 95% hafnium diboride powder with a particle size of less than 2 μm, 4% aluminum oxide with a particle size of less than 1 μm, and 1% carbon powder, and mix it with a phenolic resin solution with an alcohol content of 50% at a ratio of 100:10 Mix evenly, dry at 80°C and make 100μm granulated powder, isostatically press at a pressure of 150Mpa and keep the pressure for 30 minutes to make high-purity alumina continuous melting furnace. The billet is then demolded and fired at 2000°C for 2 hours to make a cylinder with a height of 50mm and a diameter of ?50mm. The inner cavity is a cylindrical funnel. The upper part of the cylindrical funnel is ? , The lower diameter of the cylindrical funnel is a high-purity alumina continuous melting furnace with a diameter of ?5mm.
[0016] The purity of the batching raw materials used in the experiment is industrial pure.
Embodiment 2
[0018] Mix 89% of hafnium diboride powder with a particle size of less than 2 μm, 8% of aluminum oxide with a particle size of less than 1 μm, and 3% of carbon powder, and mix it with a phenolic resin solution with an alcohol content of 50% at a ratio of 100:10 Mix evenly, dry at 80°C and make 200μm granulated powder, press isostatic pressing under pressure of 150Mpa and keep the pressure for 30 minutes to press into high-purity alumina continuous melting furnace feeding nozzle The green body is then demoulded and fired at 1800°C for 2.5 hours to make a cylinder with a height of 75mm and a diameter of ?150mm. The inner cavity is a cylindrical funnel. The upper diameter of the cylindrical funnel is ? The feeding nozzle for the high-purity alumina continuous melting furnace with a diameter of ?7mm at the lower part of the cylindrical funnel.
[0019] The purity of the batching raw materials used in the experiment is industrial pure.
Embodiment 3
[0021] Mix 78% of hafnium diboride powder with a particle size of less than 2 μm, 17% of aluminum oxide with a particle size of less than 1 μm, and 5% of carbon powder, and mix it with a phenolic resin solution with an alcohol content of 50% at a ratio of 100:10 Mix evenly, dry at 80°C and make 300μm granulated powder, isostatically press at a pressure of 150Mpa and hold the pressure for 30 minutes to press into a high-purity alumina continuous melting furnace feeding nozzle The green body is then demoulded and fired at 1600°C for 3 hours to make a cylinder with a height of 100mm and a diameter of ?200mm. The inner cavity is a cylindrical funnel. The upper diameter of the cylindrical funnel is ? Feeding nozzle for high-purity alumina continuous melting furnace with a diameter of ?10mm at the lower part of the cylindrical funnel.
[0022] The purity of the batching raw materials used in the experiment is industrial pure.
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