Suction filtration device and filtering method thereof

A suction filter device and suction filter technology, applied in the direction of filtration separation, separation methods, chemical instruments and methods, etc., can solve the problems of difficult filtration, crystal precipitation, etc., and achieve the effect of easy disassembly and cleaning

Inactive Publication Date: 2015-03-18
JIANGXI RARE EARTH & RARE METALS TUNGSTEN GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a suction filter device and a filtering method for filtering a solution and separating solid and liquid, which is beneficial to solve the influence of external factors on the solution itself in the filtering process, and is beneficial to solve the problem of Due to changes in the external environment, crystals are precipitated from the solution, resulting in difficulty in filtration

Method used

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  • Suction filtration device and filtering method thereof
  • Suction filtration device and filtering method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Example 1 like figure 1 Shown: a suction filtration device for preparing ammonium heptamolybdate with a negative pressure-resistant reactor, the common reactor 1 communicates with the negative-pressure-resistant reactor 6 through the infusion tube 3, and the negative-pressure-resistant reactor 6 communicates with the vacuum-resistant reactor 6 through the suction pipe 13 The vacuum unit 7 is connected, and the connecting pipe 8 is connected with the infusion pipe 3; the ordinary reactor 1 is equipped with a 1# stirring device 2 and a heating and heat preservation device, and the negative pressure resistant reactor 6 is equipped with a 2# stirring device 10 and a pressure gauge 5, which are movable. The inlet of the suction filter 4 under the common reactor 1 liquid level is connected with the outlet of the connecting pipe 8 .

[0016] The suction filter 4 is made up of a filter screen frame 14 and a filter cloth 9 wrapping the outer layer of the filter screen frame 14...

Embodiment 2

[0018] Example 2 like figure 2 Shown: a suction filter device with a liquid lifter for preparing high-concentration ammonium molybdate solution, the common reaction kettle 1 is connected to the liquid lifter 15 through the infusion pipe 3, and the liquid lifter 15 is connected to the vacuum unit 7 through the suction pipe 13 , the connecting pipe 8 communicates with the infusion pipe 3;

[0019] The suction filter 4 is made up of a porous filter screen frame 14 and a filter cloth 9 wrapping the outer layer of the filter screen frame. An infusion tube valve 11 is installed on the infusion tube 3 , and an inhalation tube valve 12 is installed on the inhalation tube 13 . The bottom of the liquid lifter 15 is provided with a lower valve 16 .

Embodiment 3

[0020] Example 3 like figure 1 Shown: adopt the filtration method of suction filter device described in embodiment 1 as follows:

[0021] The production process of ammonium heptamolybdate: using ammonium tetramolybdate and ammonia water as raw materials, add ammonium tetramolybdate to a certain concentration of ammonia water to dissolve, assist with stirring and heating, when the specific gravity, temperature and pH value of the solution reach a certain value When the dissolved ammonium molybdate solution is filtered, and then the solution is cooled, the ammonium heptamolybdate will be precipitated from the ammonium molybdate solution; when the crystals are precipitated to a certain extent, the solution is filtered to obtain the ammonium heptamolybdate product.

[0022] Adopting the described filtering method of embodiment 1 is: configure the high-concentration ammonium molybdate solution that meets the requirements in common reactor 1 mile, open 1# stirring device 2, 2# sti...

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Abstract

The invention relates to a suction filtration device and a filtering method thereof. An ordinary reaction kettle is communicated with a negative pressure-resistant reaction kettle or a transfer tank through a liquid conveying pipe and a connecting pipe; the negative pressure-resistant reaction kettle or the transfer tank is communicated with a vacuum set through an air suction pipe; an inlet of a suction filter movably installed under the liquid level of the ordinary reaction kettle is connected with an outlet of the connecting pipe; the suction filter comprises a porous filter screen holder and filter cloth enwrapping the outer layer of the filter screen holder; and a high-concentration ammonium molybdate solution is cooled and crystallized in the negative pressure-resistant reaction kettle and filtered and dried to obtain an ammonium heptamolybdate product, or pretreated mother liquor in the upper layer of the ordinary reaction kettle is filtered by the suction filter and is sucked into the transfer tank through the connecting pipe and the liquid conveying pipe to obtain pure high-concentration ammonium molybdate liquid. Through the suction filtration device and the filtering method thereof which are used for filtering a solution and separating a solid from liquid, the problem of filtering difficulty caused by crystal separation from the solution due to influence of external factors on the solution or change of external environment in a filtering process can be easily overcome.

Description

technical field [0001] The invention relates to a suction filtration device and a filtration method for filtering solution. The suction filter of the suction filter is completely submerged in the medium to be filtered. Background technique [0002] According to the difference in the properties of the solution system that requires solid-liquid separation, the filtration method is usually one of plate and frame filter press, vacuum suction filter, centrifugal filter, and resin layer filter. The common feature of these filtration methods is that the medium to be filtered is transferred from a container to the filter device in a certain way, the filtered solution is stored in another container, and the solid phase is accumulated in the solid-liquid separation equipment. Then it is cleared and circulated in this way to achieve the effect of solid-liquid separation. [0003] When the solid-liquid mixture to be separated is transferred from one container to another, due to the dif...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D35/02C01G39/00
Inventor 冷怀恩徐双刘剑
Owner JIANGXI RARE EARTH & RARE METALS TUNGSTEN GRP
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