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Full-automatic production process of lithium iron phosphate and devices thereof

A technology of lithium iron phosphate and production process, which is applied in the field of fully automatic production process and equipment of lithium iron phosphate, can solve problems such as poor stability between product batches, low production efficiency, increased production cost, etc., and achieves improved quality and work efficiency, increase production capacity, and reduce production costs.

Inactive Publication Date: 2015-04-22
宜春天赐高新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, existing manufacturers all adopt discontinuous production methods, and a large number of manual operations are used between processes. First, the stability between product batches is not good and the performance is unstable; second, the production cost is increased, and the production efficiency is low. ; The third is that the material flow is not in a closed condition, and the dust pollution is serious; the fourth is that the energy consumption is large, which is not conducive to energy saving and emission reduction

Method used

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  • Full-automatic production process of lithium iron phosphate and devices thereof
  • Full-automatic production process of lithium iron phosphate and devices thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Example 1: lithium carbonate (purity 99.6 wt %), ferrous oxalate (purity 99.5 wt %), ammonium dihydrogen phosphate (purity 99.2 wt %), glucose (purity 99.6 wt %), titanium dioxide (purity 99.9 wt %) Add the raw material bin, send it to the weighing and batching device through the conveyor, and automatically measure according to lithium carbonate 236kg, ferrous oxalate 1163kg, ammonium dihydrogen phosphate 724kg, glucose 108kg, titanium dioxide 10kg, then add the mixing bin, and then open the control valve through Vacuum transport to the dispersing tank filled with protective nitrogen, connect the deionized water control valve, add 2739L deionized water, start the stirring and emulsifying machine, so that the slurry is fully mixed evenly; Connect the coarse mill and the diaphragm pump to the emulsifier, control the speed of the ball mill to 800 rpm, and circulate the grinding for 6 hours under the protection of nitrogen; when the online particle size detection slurry part...

Embodiment 2

[0038] Example 2: lithium carbonate (purity 99.6wt %), iron oxide (purity 97.0wt %), ammonium dihydrogen phosphate (purity 99.0wt %), glucose (purity 99.7wt %), magnesium oxide (purity 99.5wt %) Add the raw material bin, send it to the weighing and batching device through the conveyor, automatically measure according to 236kg of lithium carbonate, 506kg of iron oxide, 724kg of ammonium dihydrogen phosphate, 108kg of glucose, and 12.6kg of magnesium oxide, then add to the mixing bin, and then open the control valve Transport to the dispersing tank by vacuum, connect the deionized water control valve, add 2739L deionized water, start the stirring and emulsifying machine, so that the slurry is fully mixed evenly; Connect the power supply of the coarse mill and the diaphragm pump, control the speed of the ball mill to 800 rpm, and circulate the grinding for 6 hours; when the particle size D50 of the slurry is about 1.0-2.0 μm through the online particle size test, start the control...

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Abstract

The invention discloses a full-automatic production process of lithium iron phosphate and the devices thereof, and belongs to the production technology field of positive materials of lithium-ion batteries. The full-automatic production process comprises the following steps of burdening, grinding, drying, roasting, crushing, packaging and the like, and is carried out in the full-automatic production process devices. The whole production process in the invention is controlled by the PLC (programmable logic controller) and is full-automatic and continuous, thus avoiding the manual operation, improving the consistency and stability of the products greatly, and enhancing the quality and work efficiency of the products; through adopting the totally enclosed type devices, the transmissions of materials among the devices are all completed in a sealed condition, and through adopting the protection from the inert atmosphere, the pollution from outside such as dust and the like is efficiently prevented, the loss and deterioration of materials in the whole process are reduced, and the quality of the products is improved; and the production method is low in energy consumption, high in capacity and continuous, reduces the production cost, and is suitable for industrial production.

Description

technical field [0001] The invention belongs to the technical field of production of positive electrode materials for lithium ion batteries, and in particular relates to a fully automatic production process and equipment for lithium iron phosphate. Background technique [0002] Lithium iron phosphate is an emerging material that has triggered a revolution in the lithium battery industry. Due to its own advantages, lithium iron phosphate batteries are widely used in various fields such as hybrid vehicles, electric vehicles, electric tools, electric bicycles, electric mopeds, and power generation and energy storage devices. . Hybrid electric vehicles (HEV) will be the main development direction of new energy vehicles in the next few years. With the continuous increase in the production of hybrid electric vehicles and the increase in the share of hybrid electric vehicles, the market size of lithium iron phosphate batteries will grow rapidly. At present, the synthesis method of...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01M4/58C01B25/45
CPCY02E60/10
Inventor 赵杰李正斌
Owner 宜春天赐高新材料有限公司
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