Full-automatic production process of lithium iron phosphate and devices thereof
A technology of lithium iron phosphate and production process, which is applied in the field of fully automatic production process and equipment of lithium iron phosphate, can solve problems such as poor stability between product batches, low production efficiency, increased production cost, etc., and achieves improved quality and work efficiency, increase production capacity, and reduce production costs.
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Embodiment 1
[0036] Example 1: lithium carbonate (purity 99.6 wt %), ferrous oxalate (purity 99.5 wt %), ammonium dihydrogen phosphate (purity 99.2 wt %), glucose (purity 99.6 wt %), titanium dioxide (purity 99.9 wt %) Add the raw material bin, send it to the weighing and batching device through the conveyor, and automatically measure according to lithium carbonate 236kg, ferrous oxalate 1163kg, ammonium dihydrogen phosphate 724kg, glucose 108kg, titanium dioxide 10kg, then add the mixing bin, and then open the control valve through Vacuum transport to the dispersing tank filled with protective nitrogen, connect the deionized water control valve, add 2739L deionized water, start the stirring and emulsifying machine, so that the slurry is fully mixed evenly; Connect the coarse mill and the diaphragm pump to the emulsifier, control the speed of the ball mill to 800 rpm, and circulate the grinding for 6 hours under the protection of nitrogen; when the online particle size detection slurry part...
Embodiment 2
[0038] Example 2: lithium carbonate (purity 99.6wt %), iron oxide (purity 97.0wt %), ammonium dihydrogen phosphate (purity 99.0wt %), glucose (purity 99.7wt %), magnesium oxide (purity 99.5wt %) Add the raw material bin, send it to the weighing and batching device through the conveyor, automatically measure according to 236kg of lithium carbonate, 506kg of iron oxide, 724kg of ammonium dihydrogen phosphate, 108kg of glucose, and 12.6kg of magnesium oxide, then add to the mixing bin, and then open the control valve Transport to the dispersing tank by vacuum, connect the deionized water control valve, add 2739L deionized water, start the stirring and emulsifying machine, so that the slurry is fully mixed evenly; Connect the power supply of the coarse mill and the diaphragm pump, control the speed of the ball mill to 800 rpm, and circulate the grinding for 6 hours; when the particle size D50 of the slurry is about 1.0-2.0 μm through the online particle size test, start the control...
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