Three-ingredient eutectic ionic liquid and preparation method thereof
An ionic liquid, eutectic technology, used in the preparation of urea derivatives, chemical instruments and methods, preparation of organic compounds, etc., can solve the problems of less research on anionic functionalization, increase in compound viscosity, etc., and achieve melting point and viscosity. Low, short response time, high stability effect
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Embodiment 1
[0024] 0.59 g (0.01 mol) of acetamide (AA), 1.36 g (0.01 mol) of ZnCl 2 Mix it with 1.74 g (0.01 mol) of 1-butyl-3-methylimidazole chloride, heat to 100°C, and keep it for 3 hours to form a colorless transparent clear liquid to obtain the ionic liquid [Bmim][Zn(AA)Cl 3 ]. It is a colorless transparent liquid at room temperature (20°C).
Embodiment 2
[0026] 0.60 g (0.01mol) urea, 1.36 g (0.01mol) ZnCl 2 , mixed with 1.74 g (0.01 mol) of 1-butyl-3-methylimidazole chloride and heated, microwave heated to 140 ° C, a colorless transparent liquid was formed, kept for 2 hours, and the ionic liquid [Bmim][Zn(Urea)Cl was obtained 3 ]. It is a colorless transparent liquid at room temperature (20°C).
Embodiment 3
[0028] 1.20 grams (0.02mol) of urea, 2.25 grams (0.01mol) of ZnBr 2 , and 2.19 grams (0.01mol) of 1-butyl-3-methylimidazole bromide were mixed and heated, heated to 110°C by microwave to form a colorless transparent liquid, and kept for 2 hours to obtain the ionic liquid [Bmim][Zn(Urea) 2 Br 3 ]. It is a colorless transparent liquid at room temperature (20°C).
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