46results about How to "Adjust conductivity" patented technology

The invention relates to a method for coating an even and controllable deposit carbon layer on the surface of LiFePO4 particles serving as lithium ion battery cathode materials for increasing the LiFePO4 conductivity. The method adopts the concrete preparation processes that: LiFePO4 powders are placed in a constant temperature zone of a chemical vapor deposition furnace, then the air in the furnace is fully discharged for inputting inert gases, after the temperature rises to the set level, a carbon source gas is input for covering a conductivity carbon film on the surface of the LiFePO4 particles evenly, the LiFePO4 coated with the carbon film has excellent conductivity which is increased by five orders of magnitude compared with the condition before coating. The chemical vapor deposition temperature ranges from 580 to 720DEG C, the deposition time is from 1 to 10 hours, and the volume percent of the carbon source gas is between 1 and 20 percent, and a sample deposited with carbon is cooled to the room temperature with a natural furnace and is then taken out. The method can cover the conductivity carbon film on the surface of each LiFePO4 particle evenly for increasing the conductivity of LiFePO4, and the thickness of the conductivity carbon film can be accurately controlled in the range of 2 to 50 nanometers through adjusting parameters (deposition temperature, deposition time and carbon source gas volume percent) of the chemical vapor deposition process.

The invention discloses a method for preparing electrically conductive hydrogel. The method includes steps of (1), uniformly dispersing hydrophilic monomers or hydrophilic polymers in hydrochloric acid aqueous solution to obtain stable dispersion liquid, adding electrically conductive monomers and metal alkoxide into the dispersion liquid and uniformly stirring the electrically conductive monomers, the metal alkoxide and the dispersion liquid; (2), adding initiators and catalysts into mixed liquid obtained at the step (1), uniformly mixing the initiators, the catalysts and the mixed liquid with one another and then carrying out reaction at the temperature ranging from -20 DEG C to 50 DEG C for 24-72 hours. The electrically conductive hydrogel can be obtained after the reaction is completely carried out. The mass of the electrically conductive monomers is 1-20% of the mass of the hydrochloric acid aqueous solution, is 20-100% of the mass of the metal alkoxide and is 0.2-85% of the massof the hydrophilic monomers or the hydrophilic polymers. The mass of the initiators is 0.5-5% of the mass of the electrically conductive monomers, and the mass of the catalysts is 0.01-5% of the massof the hydrophilic monomers. Compared with existing methods, the method has the advantages that the electrically conductive hydrogel prepared by the aid of the method is excellent in mechanical property and electrochemical performance and can be prepared at one step, and the method includes simple processes for preparing the electrically conductive hydrogel and is low in raw material usage.

The invention discloses a preparation method of controllable nitrogen-doped carbon nanotubes. The method comprises the following steps: dissolving a metal salt, a carbon source and a nitrogen source in an aqueous or ethanol solution, performing stirring at 60-80 DEG C until the solution volatilizes to form a sol, drying the sol at 80-120 DEG C to form a gel, carrying out high-temperature heat treatment carbonization on the above gel precursor, keeping the temperature at 350-650 DEG C for 2-4 h, keeping the temperature at 750-1000 DEG C for 5-10 h to obtain nitrogen-doped carbon nanotubes containing metal or metal sulfide, and simply corroding the nitrogen-doped carbon nanotubes containing metal or metal sulfide to obtain the nitrogen-doped carbon nanotubes. The above sol-gel technology canrealize the effective regulation of the caliber and the length of the nitrogen-doped carbon nanotubes and the adjustment of the nitrogen content, the pore structure and the conductivity of the nitrogen-doped carbon nanotubes. The nitrogen-doped carbon nanotubes can effectively prolong the cycle life of a battery when applied to the electrode material of the battery, has good electrochemical performances, and is hopeful to be applied to fields of electrochemical catalysis, energy transition and energy storage.

The invention relates to the field of functional composite materials, in particular to an ultra-high molecular weight polyethylene-graphene-nickel composite material with a high electromagnetic shielding performance and a preparation method. Composite materials used for preparing the composite materials are nickel-plated graphene-coated ultra-high molecular weight polyethylene particles taking metallic nickel as a shell structure and taking graphene-coated ultra-high molecular weight polyethylene particles as a core, wherein the content of the graphene-coated ultra-high molecular weight polyethylene particles ranges from 97.42 vol% to 98.91 vol%, the content of metallic nickel ranges from 1.09 vol% to 2.58 vol%, and the content of graphene in the composite material is at least 0.028 vol%. By preparing the composite material with the isolation structure, on the condition that the content the metallic nickel and the content of the graphene are extremely low, the electric conductivity and electromagnetic shielding performance of the composite material can be significantly improved, and the purposes of the high electric conductivity and the high electromagnetic shielding performance of the composite material are achieved.

The invention discloses a method for preparing low-cost low-temperature cured conductive paste for screen printing. In the preparation method, base metal nickel (Ni) is used to replace part of used precious metal silver (Ag); nickel powder and silver powder form a conductive function phase of the conductive paste together, wherein the change of the adding proportion of the nickel powder not only can adjust the final electrical property, but also can adjust the printing performance of the paste well; the change of the adding proportion of an organic carrier can adjust the viscosity and the electric conductivity of a product; and the change of the adding proportion of a thickening agent can adjust the viscosity, the leveling property and the printing performance of the product. The quick drying and curing can be performed at a constant temperature of between 120 and 150 DEG C to form the product with good electrical property. The conductive paste of the invention adopts the base metal to replace partial precious metal silver, so the production cost is greatly reduced, and the performance reaches the level of high silver content.

The invention relates to a preparation method for tin oxide-doped composite conductive powder using kaolinite as base material. The invention is characterized in that dispersing agent is mixed with kaolinite ore to produce homogeneous and dispersed suspended ore slurry; chemical co-precipitation method is adopted for homogeneous precipitation in the form of hydroxide or hydrous oxide, then the composite conductive powder is obtained after filtering, washing, gas-liquid separation, calcination and grinding of precipitation products. The invention has the advantages of greatly reduced preparation cost of conductive powder, greatly improved use value of kaolinite resources, easy dispersion of the composite conductive powder, stable quality, light powder color, good conductivity, conductive additives for various colors (such as white) and wide application prospect.

The invention discloses a composite conductive powder containing barium sulfate, which comprises a powder containing barium sulfate. The surface of the powder containing barium sulfate is coated with tin dioxide and antimony trioxide. The composite conductive powder containing barium sulfate in the invention is characterized by small particle size, high white degree, good dispersion, good conductivity, low production cost, simple process and fitness of industrial production.

The invention relates to sintered flux for nickel strip electrode electro-slag welding. The sintered flux for the nickel strip electrode electro-slag welding is characterized in that the intered flux is prepared from dry powder components and binder water glass; the dry powder components comprise, by mass, 45-75% of CaF2, 15-35% of Al2O3, 1-5% of SiO2, 1-5% of CaO, 1-5% of MgO, 1-10% of sodium fluoroaluminate, 1-5% of rare earth fluoride and 1-5% of ferroniobium alloy powder; the ratio of potassium to sodium of the binder water glass is 1 to 1, the molar ratio is 2.2-3.5, the baume degree at room temperature is 38-50, and the dosage is 15-25% of the weight of the dry powder. The sintered flux can be used through being matched with various nickel base welding strip such as EQNiCrMo-3 and EQNiCr-3, when strip electrode electro-slag surfacing is conducted through matching with the nickel base welding strip, stable electro-slag process and welding technological property can be maintained at the quick welding condition of 250 mm/min, the quality of formation of surfacing layers is good, defects do not exist in lap joint, and various indexes of the surfacing layers can meet usage requirements of users.

The invention provides an electrochemical power supply diaphragm and a manufacturing method thereof. The method includes the steps that polyvinylidene fluoride-hexafluoropropylene is dissolved in acetone to prepare a polyvinylidene fluoride-hexafluoropropylene acetone solution with the mass concentration of 5-20%, then deionized water is added into the solution, and the mixture is uniformly stirred to obtain emulsion; the mass content of the deionized water in the emulsion is 1-10%; organic short fibers are added into the emulsion, and the mixture is uniformly mixed to obtain mixed emulsion; the obtained mixed emulsion is coated on a clean glass substrate, the glass substrate is removed after the mixed emulsion is dried, and accordingly the electrochemical power supply diaphragm is obtained. The organic short fibers are one or more of PET fibers, PAN fibers and aramid fibers. The electrochemical power supply diaphragm is proper in aperture and good in heat resistance and safety, and safety of an electrochemical battery or a capacitor can be effectively improved. The invention further provides the electrochemical battery or the capacitor using the diaphragm.

The invention discloses an Ag-Cu alloy in-situ fibre composite material with high strength, high electrical conductivity and low Cu content and a preparation technology thereof. The Cu content of thecomposite material is equal to or less than 20% by weight percent; the in-situ fiber composite material is formed by utilizing Ag-Cu alloy eutectic structure and adopting great deformation and reasonable heat treatment technology. The preparation technology comprises the following steps: pouring Ag-Cu alloy in the protective atmosphere after vacuum smelting; carrying out hot extrusion, ageing preheat treatment, cold large strain processing, intermediate heat treatment and stabilizing heat treatment to manufacture Ag-Cu composite material with strengthened Cu fiber in the dimensions of micron,submicron or nanometer. Composite material with optimal combination of tensile strength and electrical conductivity performance can be obtained by optimizing various technological parameters in the manufacturing process. The highest performance can reach that the ultimate tensile strength UTS is equal to or greater than 1GPa, and the relative electrical conductivity is equal to or greater than 60%IACS. The Ag-Cu in-situ composite material can be used as conducting material with high strength and high electrical conductivity.

The invention belongs to the technical field of electrode materials, and particularly relates to a rare earth doped lithium titanate electrode material and a preparation method thereof. The preparation method for the rare earth doped lithium titanate electrode material comprises the following steps that: firstly, mixing titanium dioxide, lithium carbonate, rare earth compound and carbohydrate in solvent to prepare slurry; drying the slurry; under an inert atmosphere, a reduction atmosphere or a vacuum atmosphere, carrying out first-stage calcination; and under an oxidization atmosphere, carrying out second-stage calcination to prepare the rare earth doped lithium titanate electrode material. The rare earth doped lithium titanate electrode material prepared with the preparation method has excellent characteristics, including high multiplying power performance, good cycling stability, quick charging and discharging capability and the like. In addition, the preparation method is simple and can carry out batch preparation.

The invention relates to a tunable array integrated broadband terahertz wave-absorbing resonator based on vanadium dioxide. The tunable array integrated broadband terahertz wave-absorbing resonator comprises a metal reflecting layer, a middle dielectric layer, a vanadium dioxide phase change layer, a graphene adjustable conductivity layer, a top conductive electrode and metal resonant cavities which are arranged in a periodic array from bottom to top. According to the metal resonant cavity, specific geometric parameters and structures are designed, so that the whole metamaterial wave-absorbing structure generates electromagnetic resonance at a specific frequency, and the wave-absorbing structure with relatively high modulation depth is designed by utilizing the thermally induced phase change property of vanadium dioxide and the huge change of optical and electrical parameters in a semiconductor phase state and a metal phase state; and based on the adjustable conductivity property of graphene, the Fermi level of graphene is changed through external voltage, and the dielectric parameters of the wave absorbing structure are changed, so that the absorption wavelength range is changed. By combining the tuning characteristics of the two materials, the broadband absorber is actively tuned through heat/electricity, and the designed structure is compatible with the process and is easy to implement.

The invention discloses a double-component rapid low-temperature curing conductive adhesive which comprises the following components in parts by mass: a conductive adhesive component A and a conductive adhesive component B, wherein the conductive adhesive component A comprises 180-200 parts of silver-plated copper powder, 100 parts of epoxy resin and 10-15 parts of a reactive diluent; the conductive adhesive component B comprises 180-200 parts of silver-plated copper powder, 10-15 parts of a reactive diluent, 20-30 parts of a curing agent, 10-20 parts of an accelerator and 5 parts of a leveling agent or a defoaming agent. As copper powder is plated with silver for three times innovatively, copper powder with a high-density silver layer can be prepared. The silver-plated copper powder can be applied to the conductive adhesive, then the double-component rapid low-temperature curing conductive adhesive can be prepared, and meanwhile a conductor prepared from the conductive adhesive applied to a substrate is high in conductivity and good in mechanical strength.

The invention discloses an acoustic surface wave type humidity sensor based on conductive polymer composite nano-fibre and a preparation method thereof. The acoustic surface wave type humidity sensor is prepared by depositing polyaniline and polyvinyl butyral composite nano-fibre on an acoustic surface wave device by adopting an electrostatic spinning method. The acoustic surface wave type humidity sensor has good response linearity and rapid response in a wide humidity range and also has high response sensitivity of being up to 75 kHz/%RH. For low-humidity detection, the acoustic surface wave type humidity sensor also has higher sensitivity and response linearity and is capable of detecting 0.5%RH extra-low humidity. The preparation method disclosed by the invention is simple, convenient and easy to do; the prepared acoustic surface wave type sensor can be widely applied to detecting and controlling environmental humidity in industrial and agricultural production, storage, weathers and daily lives; and signal wireless and remote transmission can be conveniently realized.

The invention discloses a preparation method of a copper-aluminum layered composite material capable of effectively controlling interface reaction. The method comprises the following steps: 1, preparing GO/Al foil; 2, sequentially and alternately placing the dried GO/Al foil and the Cu foil subjected to surface pretreatment in an overlapped mode in the direction of a tiled layer, and obtaining a Cu-GO/Al prefabricated body; 3, pressurizing the Cu-GO/Al prefabricated body, then heating, and carrying out heat preservation and pressure maintaining; and 4, cooling and decompressing to obtain the copper-aluminum layered composite material. The preparation method comprises the following steps: stacking GO/Al foil with GO deposited on the surface and Cu foil, and then heating and pressurizing forpressing; the GO between the Cu foil and the Al foil is used for preventing Cu and Al from reacting at the interface to form an intermetallic compound; the Cu-Al interface reaction combination condition in the copper-aluminum layered composite material is improved, meanwhile, the heat conduction performance and the electric conduction performance of the copper-aluminum layered composite materialare guaranteed, and the structural function integrated design of the copper-aluminum layered composite material is achieved.

The invention relates to a high-toughness and low-resistivity silver-gold alloy bonding wire. The high-toughness and low-resistivity silver-gold alloy bonding wire is prepared from the alloy components in percentage by weight: 80%-100.0% of Ag, 0%-20.0% of Au, and 0%-0.01% of two or more of Ce, Cu, Pd, Be, Mg and Ca which are minute in content. According to the high-toughness and low-resistivity silver-gold alloy bonding wire, the fracturing load is larger than 10 cN, meanwhile the elongation is larger than 18%, the mechanical property is adjustable and controllable, and the resistivity is smaller than 1.8 [mu]omega.cm; and the using cost of the silver-gold alloy bonding wire is lowered by 80% or above compared with the material cost of an existing bonding alloy wire, the mechanical property, the electrical property, oxidation resistance and the bonding property are excellent, and thus the high-toughness and low-resistivity silver-gold alloy bonding wire can be widely applied to the field of packaging.

The invention discloses a saline soil improvement agent and a saline soil improvement method. The improvement agent is prepared from, by mass, 70-80 parts of garden waste compost, 10-15 parts of fluegas desulfurization gypsum, 5-6 parts of ammonium sulfate and 10-12 parts of a 1% emulsifier OP-10 solution. The saline soil improvement method comprises the following steps of composting and decomposition treatment, saline soil ploughing, improvement agent mixing and preparation, improvement agent covering for saline soil and mixed turning. The improvement agent can reduce the pH of coastal saline soil, regulate the conductivity of the saline soil, increase soil nutrients, increase the plant biomass, and increase the nutrient content in plants.

The invention discloses a preparation method of a cellulose nano-whisker/graphene flexible transparent conductive film. Tea-oil tree shell is taken as the raw material, and tea-oil tree shell cellulose nano-whiskers are obtained by separation through the main steps of cooking through an alkali method, alkali treatment, purification, bleaching, acidolysis, centrifuging, dispersing and the like; theobtained cellulose nano-whiskers are large in specific surface area, high in Young modulus and high in reactivity; next, suction filtration is performed to obtain a substrate film which is uniform and smooth in surface, and relatively high in flexibility, light transmission, mechanical property and thermodynamic property; by taking graphene as a conductive matrix, and under the effect of CTAB, the graphene is uniformly paved on the surface of the substrate film through a suction filtration method to form a uniform and a continuous conductive layer; and by controlling the adding amount of graphene and the number of layers of graphene on the surface of the film, the prepared flexible transparent conductive film has relatively high flexibility, foldable property, elasticity, rigidity and thermal stability and bright application prospect.

A magnetically-conductive alignable nano-sheet silver paste comprising nano-sheet silver particles, wherein the nano-sheet silver particles are nano-thick film sheets having a structure of silver-alloy-silver, wherein the single layer thickness of the silver is 5 to 20 nm; The thickness of the single layer of the alloy is 5-20nm; The total thickness of the nanosheet silver particles is 15 to 60 nm, and the particle size (d50) is 0.3 to 1. M u.m. Compared with the prior art, the nano-sheet silver paste has the following beneficial effects: the multi-element alloy in the nano-sheet silver particles has magnetic conductivity, and the nano-sheet silver is arranged in a regular manner under the guidance of a magnetic mode, so that the shape advantage of the nano-sheet silver is fully brought into play, and a nano-sheet silver paste with high electric conductivity is obtained.

The invention discloses an electrode boiler device which comprises a boiler body, a drain outlet formed in the bottom end of the boiler body, a circulating water outlet and a water outlet in the side face of the bottom, a second thermometer on the inner side of the bottom, a circulating water inlet in the middle bottom, a pressure gauge on the middle top, an air inlet valve and an exhaust valve on the top and an electrode at the top end. A three-way valve and an electrode of the circulating water inlet are connected to the inner furnace, a pressure difference transmitter and a first thermometer are arranged at the bottom end of the inner furnace, and a drainage valve is arranged at the protruding position of the bottom end of the inner furnace. The pressure, temperature, water level, power and solution conductivity can be adjusted, and the electrode reaction area and the height of the inner furnace can be adjusted.