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High-content glass fiber reinforced material with low mold scale and excellent surface quality and preparation method thereof

A technology with high glass fiber content and surface quality, applied in the field of resin and its preparation, can solve the problems that PBT materials cannot provide low-fouling solutions, and achieve the effect of excellent surface, good mechanical properties and broad application prospects

Active Publication Date: 2016-08-10
SHANGHAI KUMHO SUNNY PLASTICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of this patent is to overcome the existing high glass fiber content reinforced PBT materials that cannot provide low-fouling solutions, limit the surface defects of PBT resins with high-content glass fiber additions, and provide a low mold fouling and excellent surface quality. High-content glass fiber reinforced material and its preparation method

Method used

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  • High-content glass fiber reinforced material with low mold scale and excellent surface quality and preparation method thereof
  • High-content glass fiber reinforced material with low mold scale and excellent surface quality and preparation method thereof
  • High-content glass fiber reinforced material with low mold scale and excellent surface quality and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] The low mold fouling and high-content glass fiber reinforced material with excellent surface quality in this example, the components contained and the parts by weight of each component are shown in Table 1, and the preparation method is as follows:

[0033] (1) Take each raw material according to the parts by weight shown in Table 1;

[0034] (2) Dry the PBT resin at 120-140°C for 5 hours;

[0035] (3) PBT resin, nucleating agent, toughening agent Elvaloy PTW, antioxidant and processing aid are mixed evenly and placed in a twin-screw extruder, and glass fiber compound is added downstream of the extruder, and finally passed Screw conveying, shearing and kneading, material melting and compounding, and then extrusion, drawing, low-temperature cooling and pelletizing to obtain products.

[0036] The feeding speed of the twin-screw extruder is controlled at 350-450rpm, the temperature of each partition is kept at 200-245°C, the screw speed is 350-450rpm, and the vacuum pump...

Embodiment 2

[0038] The low mold fouling and high-content glass fiber reinforced material with excellent surface quality in this embodiment, the components contained and the parts by weight of each component are shown in Table 1, and the preparation method is as follows:

[0039] (1) Take each raw material according to the parts by weight shown in Table 1;

[0040] (2) Dry the PBT resin at 120-140°C for 5 hours;

[0041] (3) PBT resin, toughening agent, antioxidant, nucleating agent and processing aid are mixed evenly and placed in the twin-screw extruder, and the glass fiber compound is added downstream of the extruder, and finally passed through the screw Conveying, shearing and mixing, melting and compounding of materials, and then extruding, drawing, cooling at low temperature and pelletizing to obtain products.

[0042]The feeding speed of the twin-screw extruder is controlled at 350-450rpm, the temperature of each partition is maintained at 200-245°C, the screw speed is 350-450rpm, ...

Embodiment 3

[0044] The low mold fouling and high-content glass fiber reinforced material with excellent surface quality in this example, the components contained and the parts by weight of each component are shown in Table 1, and the preparation method is as follows:

[0045] (1) Take each raw material according to the parts by weight shown in Table 1;

[0046] (2) Dry the PBT resin at 120-140°C for 5 hours;

[0047] (3) PBT resin, toughening agent, antioxidant and auxiliary agent are mixed uniformly and placed in a twin-screw extruder, and alkali-free glass fiber HP3786 is added downstream of the extruder, and finally conveyed, sheared and Kneading, melting and compounding of materials, and then extruding, drawing, cooling at low temperature, and pelletizing to obtain products.

[0048] The feeding speed of the twin-screw extruder is controlled at 350-450rpm, the temperature of each partition is maintained at 200-245°C, the screw speed is 350-450rpm, and the vacuum pump on the twin-scre...

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Abstract

The invention discloses a low-mold-deposit high-surface-quality high-content glass fiber reinforced material and a preparation method thereof. The glass fiber reinforced material comprises the following components in parts by weight: 30-60 parts of polybutylene terephthalate, 30-60 parts of glass fiber, 0-10 parts of reactive toughener, 0.1-2 parts of nucleating agent, 0.2-0.6 part of antioxidant and 0.5-1 part of assistant. The preparation method of the glass fiber reinforced material comprises the following steps: weighing the components according to parts by weight; drying polyester resin at 90-110 DEG C for 4-6 hours; evenly mixing the polyester resin, toughener, antioxidant and assistant, adding the mixture into a double screw extruder, and adding alkali-free glass fibers downstream the extruder; and melting, compounding, extruding, cooling, drying and granulating. According to the invention, part of the glass fibers not treated by a wetting agent and the glass fibers treated by the wetting agent are compounded, and the reactive assistant is further added into the system; and thus, the product has favorable physical properties, thereby overcoming the defect that micromolecules can easily precipitate to influence the surface quality and generate mold deposit when high-content glass fibers are added.

Description

technical field [0001] The invention relates to a resin and a preparation method thereof, in particular to a high-content glass fiber reinforced material with low mold fouling and excellent surface quality and a preparation method thereof. Background technique [0002] Polybutylene terephthalate (PBT) is an increasingly widely used engineering plastic. It has comprehensive and stable mechanical properties, good hydrolysis resistance, and lower hygroscopicity than nylon and other materials. Little impact on stability; better resistance to chemicals, solvents, and weathering; faster crystallization speed than PET and other materials, good fluidity, excellent formability; high dielectric strength; low friction coefficient, wear resistance, bending creep Good performance; easy to make glass fiber reinforced and flame retardant products. [0003] Reinforced PBT is one of the earliest industrialized PBT modified products. Glass fiber reinforced PBT is currently the most important...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L67/02C08K9/00C08K7/14C08J5/08B29C47/92B29C48/92
CPCB29C48/04B29C48/40
Inventor 罗鹏李强罗明华辛敏琦
Owner SHANGHAI KUMHO SUNNY PLASTICS