Preparation method of mangrove acanthus ilicifolius extract
The technology of a mangrove plant and acanthus, which is applied in the field of preparation of mangrove plant extracts, can solve the problems of unsuitability for industrial production, complicated preparation methods, and high extraction costs, and achieve easy industrial production, high extraction rate, and low extraction cost. low effect
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[0017] Example 1
[0018] The preparation method of mangrove plant rat botanical extract includes the following steps:
[0019] 1) Raw material pretreatment: Take the whole plant of the rat bunker, wash it, drain it, and then put it in an oven, dry it at a temperature of 30 ℃, and then smash and sieve to obtain rat bunker powder with a particle size of less than 0.25mm, and set aside ;
[0020] 2) Reflux extraction: Use 70% ethanol solution for reflux extraction of the rat botanical powder obtained in step 1) for 1.5 hours each time, filter, and combine each filtrate to obtain crude extract I and residue I. Among them, the ratio of the mass of the rat abies powder to the volume of the ethanol solution is 1kg: 10L;
[0021] 3) Ultrasonic extraction again: Mix the residue I obtained in step 2) with a 70% ethanol solution, and perform ultrasonic extraction once at a temperature of 70°C for 2 hours. Filter and separate the liquid residue. Obtain crude extract II and residue II, in which...
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[0024] Example 2
[0025] The preparation method of mangrove plant rat botanical extract includes the following steps:
[0026] 1) Raw material pretreatment: Wash the roots and leaves of the rat botanical plants, drain them, put them in an oven, dry them at a temperature of 50 ℃, and then crush and sieve to obtain rat botanicals powder with a particle size of less than 0.25 mm ,spare;
[0027] 2) Reflux extraction: Use 72% ethanol solution for reflux extraction of the rat hairpin powder obtained in step 1), extraction time 2h, and filter to obtain crude extract I and residue I, of which rat hairpin powder The ratio of the mass of the material to the volume of the ethanol solution is 1kg: 8L;
[0028] 3) Ultrasonic extraction again: Mix the residue I obtained in step 2) with a 72% ethanol solution, and at a temperature of 80 ℃, ultrasonic extraction 2 times, each extraction time is 1.5h, filter, and liquid Separate the residues and combine each filtrate to obtain crude extract II and...
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[0031] Example 3
[0032] The preparation method of mangrove plant rat botanical extract includes the following steps:
[0033] 1) Raw material pretreatment: Take the leaves of the rat botanicals plant, wash, drain, and then put them in an oven, dry at a temperature of 45 ℃, and then crush and sieve to obtain rat botanicals powder with a particle size of less than 0.25 mm. spare;
[0034] 2) Reflux extraction: the rat botanical powder obtained in step 1) is refluxed and extracted twice with a 75% ethanol solution for 2 hours each time, filtered, and each filtrate is combined to obtain crude extract I and residue I. The ratio of the mass of the rattan powder to the volume of the ethanol solution is 1kg: 8L;
[0035] 3) Ultrasonic re-extraction: mix the residue I obtained in step 2) with a 75% ethanol solution, and perform ultrasonic extraction once at a temperature of 85°C for 1.5 hours, filter, and separate the liquid residue , To obtain crude extract II and residue II, in which res...
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