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Novel oxidation furnace for preparing tin dioxide

The technology of an oxidation furnace and an oxidation chamber is applied in the field of equipment for preparing tin dioxide by gas phase method, which can solve the problems of heat loss, high consumption of tin, large consumption of nitric acid, etc., and achieve the effects of saving energy consumption, reducing emissions and improving quality

Active Publication Date: 2014-08-13
GUANGXI HUAXI GRP CO LTD
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Problems solved by technology

At present, the production of tin dioxide mainly includes wet method and fire method. The wet method is mainly nitric acid method. This method consumes a lot of nitric acid, causes serious environmental pollution, high tin consumption and low product purity.
In addition, the wet method also includes sol-gel method, gel-combustion method, chemical precipitation method, etc. to produce nano-scale tin dioxide. The wet method requires drying, calcination and other processes in production, so the energy consumption is also relatively large
The current fire method is mainly the gasification method. Although it solves the problem of polluting gas in production, due to the limitation of oxidation equipment, the production is discontinuous, resulting in a large amount of heat loss and affecting the quality of the product.

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  • Novel oxidation furnace for preparing tin dioxide
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Embodiment Construction

[0015] Combine below figure 1 and figure 2 The present invention is described in further detail:

[0016] The oxidation furnace of the present invention comprises a hearth 1 and a reaction device 2 arranged in the hearth, a combustion space 11 for heating the reaction device is formed between the hearth and the reaction device, and a flue exhaust duct 12 communicating with the combustion space is provided on the hearth, The flue gas after combustion in the combustion space is directly discharged from the flue to reduce the emission of pollutants. The reaction device 2 includes an upper layer melting chamber 21 and a lower layer oxidation chamber 22, and an interlayer 23 is arranged between the oxidation chamber and the melting chamber, which prevents the oxidation chamber from being directly communicated with the melting chamber; a vertically arranged hollow rotating shaft 3 passes through the Pass through the partition, one end of which stretches out of the melting chamber...

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Abstract

The invention relates to equipment for preparing tin dioxide according to a gas-phase method, in particular to a novel oxidation furnace for preparing tin dioxide. The novel oxidation furnace comprises a reaction device, wherein the reaction device comprises a melting chamber on an upper layer and an oxidizing chamber on a lower layer; a partition layer is arranged between the oxidizing chamber and the melting chamber; a vertical hollow rotary shaft penetrates the partition layer; a charging opening communicated with the melting chamber and the hollow cavity of the rotary shaft is formed in the section, below the melting chamber, of the rotary shaft; a plurality of through holes communicated with the hollow cavity are formed in the section, above the oxidizing chamber, of the rotary shaft; oxide discharge openings are formed in both the melting chamber and the oxidizing chamber. As tin is melt and oxidized in the same hearth, energy is saved effectively; melted tin is thrown out of the through holes through the rotation of the rotary shaft and enough high-pressure gas after entering the hollow cavity, and strikes the wall of the oxidizing chamber, so that the interiors of tin drips can be oxidized till the tin drips are oxidized completely. Therefore, the quality of tin dioxide products is improved.

Description

technical field [0001] The invention relates to equipment for preparing tin dioxide by gas phase method, in particular to an oxidation furnace for preparing tin dioxide. Background technique [0002] Tin dioxide is widely used in the production of electrode materials, conductive oxide films, glass industry, electronics industry, and ceramics industry. At present, the production of tin dioxide mainly includes wet method and fire method. The wet method is mainly nitric acid method, which consumes a lot of nitric acid, causes serious environmental pollution, high tin consumption and low product purity. In addition, the wet method includes sol-gel method, gel-combustion method, chemical precipitation method, etc. to produce nano-scale tin dioxide. The wet method requires drying, calcination and other processes in production, so the energy consumption is also relatively large. The current fire method is mainly the gasification method. Although it solves the problem of polluting ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01G19/02B82Y30/00
CPCY02P20/10
Inventor 陈进中伍祥武吴伯增甘振英林东东
Owner GUANGXI HUAXI GRP CO LTD