Application of PES (polyether sulfone) microporous membrane in automatic liquid stopper
A technology of microporous film and polyethersulfone, which is applied in the direction of subcutaneous injection devices, etc., can solve the problems of low BP value, slow flow rate, poor hydrophilicity of liquid stop membrane, etc., and achieve safe and convenient infusion process, increase safety and convenience effect
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[0024] Example 1
[0025] Dissolve 10 (wt)% of the total mass of polyethersulfone in N,N-dimethylacetamide, and add 8 (wt)% of the total mass of polyvinylpyrrolidone, and stir at 25°C. It is dissolved, passed through a 200-mesh filter, and vacuum degassed to obtain a casting solution. At a temperature of 25°C, the casting liquid was scraped on the non-woven fabric to form a 0.2mm thick liquid film, and it was allowed to stand and evaporate in the air with a relative humidity of 40% for 30 seconds to form a preliminary gel. Phase inversion is carried out in a water bath containing 5 (wt)% of the total mass of N,N-dimethylacetamide gel at a temperature of 40°C to obtain a polyethersulfone microporous film.
Example Embodiment
[0026] Example 2
[0027] Dissolve 15 (wt)% of the total mass of polyethersulfone in N,N-dimethylacetamide, and add 10 (wt)% of the total mass of polyvinylpyrrolidone, and stir at 50°C. It is dissolved, passed through a 200-mesh filter, and vacuum degassed to obtain a casting solution. At a temperature of 40°C, the casting liquid was scraped on the non-woven fabric to form a 0.2mm thick liquid film, which was allowed to stand and evaporate for 120 seconds in the air with a relative humidity of 80%, and the gel was initially gelled. Phase inversion is carried out in a water bath containing 5 (wt)% of the total mass of N,N-dimethylacetamide gel at a temperature of 40°C to obtain a polyethersulfone microporous film.
Example Embodiment
[0028] Example 3
[0029] Dissolve 15 (wt)% of the total mass of polyethersulfone in N,N-dimethylacetamide, add 8 (wt)% of the total mass of polyvinylpyrrolidone, and stir at 40°C. It is dissolved, passed through a 200-mesh filter, and vacuum degassed to obtain a casting solution. At a temperature of 20°C, the casting liquid was scraped on the non-woven fabric to form a 0.3mm thick liquid film, and it was allowed to stand and evaporate for 80 seconds in the air with a relative humidity of 60% to form a preliminary gel. Phase inversion is carried out in a water bath containing 5 (wt)% of the total mass of N,N-dimethylacetamide gel at a temperature of 25°C to obtain a polyethersulfone microporous film.
[0030] The polyethersulfone microporous film prepared in Examples 1 to 3 is cut into a certain shape and then installed in the automatic liquid stopping device of the infusion set through ultrasonic welding and other processes. All of them can achieve a good automatic liquid stoppin...
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