A kind of preparation method of superfine kaolin with high oil absorption value
An ultra-fine kaolin, high oil absorption technology, applied in chemical instruments and methods, inorganic chemistry, non-metallic elements, etc., can solve the problems of low viscosity, low product quality, low technical content, etc., to achieve easy dispersion, non-corrosive viscosity Effect
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Embodiment 1
[0019] A kind of preparation method of superfine kaolin with high oil absorption value described in the present embodiment 1, comprises the following steps:
[0020] (1) Put 1000g of kaolin raw ore into a drying oven, dry at 100°C for 1.5h, take it out and use a multi-functional pulverizer to pulverize it for 10min to below 200 mesh;
[0021] (2) Take 500g of pulverized kaolin and 500ml of water to make a slurry and pour it into the big sesame cake, add 1 g of sodium dithionite and sodium polyacrylate at a weight ratio of 0.001, and stir under electric power at room temperature for 1 hour at a speed of 500 r / min; Then add 4 ml of sulfuric acid with a concentration of 98% and 20 g of hydrogen peroxide into the beaker, and continue vigorous stirring for 2 h; the volume ratio of sulfuric acid is 0.004;
[0022] (3) Using the SW-3000 wet grinding machine, pump the slurry prepared in step (2) into the grinding machine for 1 hour, and add 2 g of sodium dodecylsulfonate at a weight r...
Embodiment 2
[0027] A kind of preparation method of superfine kaolin with high oil absorption value of this embodiment 2, its steps are:
[0028] (1) Put 1000g of kaolin raw ore into a drying oven, dry at 100°C for 1.5h, take it out and use a multi-functional pulverizer to pulverize it for 10min to below 200 mesh;
[0029] (2) Take 500g of pulverized kaolin and 500ml of water to make a slurry and pour it into a large sesame cake, add 1 g of sodium dithionite and sodium polyacrylate at a weight ratio of 0.0015, and stir electrically at room temperature for 1.5 hours at a speed of 500r / min; Then add 4 ml of hydrochloric acid with a concentration of 98% and 20 g of hydrogen peroxide into the beaker, and continue vigorous stirring for 2 h; the volume ratio of hydrochloric acid is 0.005;
[0030] (3) Using the SW-3000 wet grinding machine, pump the slurry prepared in step (2) into the grinding machine for 1.5 hours, and add 2g sodium dodecylsulfonate at a weight ratio of 0.001~0.002 during the ...
Embodiment 3
[0035] The preparation method of a kind of high oil absorption superfine kaolin of this embodiment 3, its steps are:
[0036] (1) Put 1000g of kaolin raw ore into a drying oven, dry at 100°C for 1.5h, take it out and use a multi-functional pulverizer to pulverize it for 10min to below 200 mesh;
[0037] (2) Take 500g of pulverized kaolin and 500ml of water to make a slurry and pour it into a large sesame cake, add 1 g of sodium dithionite and sodium polyacrylate at a weight ratio of 0.0015, and stir electrically at room temperature for 1.5 hours at a speed of 500r / min; Then add 4 ml of sulfuric acid with a concentration of 98% and 20 g of hydrogen peroxide into the beaker, and continue stirring vigorously for 2 h; the volume ratio of sulfuric acid is 0.005;
[0038] (3) Using the SW-3000 wet grinding machine, pump the slurry prepared in step (2) into the grinding machine for 1.5 hours, and add 2g sodium dodecylsulfonate at a weight ratio of 0.001~0.002 during the grinding proc...
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