A kind of asphalt modification additive
An asphalt modifier and asphalt modification technology, which is applied in the field of asphalt modifiers, can solve the problems of insignificant changes in asphalt performance and large usage, and achieve the advantages of reducing early road diseases, decreasing penetration, and simple application process. Effect
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[0020] Embodiment 1: the preparation of formula I compound
[0021] Add 0.12mol of 4-fluorophenylbutyric acid, 0.24mol of thionyl chloride, 80ml of toluene and 0.2ml of dimethylformamide (DMF) into the reaction flask, and react at 80°C (uncorrected) for 6h. The solvent and the remaining thionyl chloride were distilled off under reduced pressure to obtain a yellow liquid, which was dissolved in 40 ml of acetone to obtain a 4-fluorophenylbutyryl chloride solution.
[0022] Add 0.1mol of 3,5-difluoro-2-hydroxy-pyridine, 100ml of acetone and 0.11mol of m-picolinic acid into the reaction flask in turn; add all the prepared 4-fluorophenylbutyryl chloride solution under ice bath, and react at room temperature 10h; filter, add 280ml (1mol / L) dilute hydrochloric acid to the filtrate, stir, crystallize, filter; the filter cake is washed successively with distilled water (50ml×2), petroleum ether 60ml, ethanol-water (ethanol:water volume ratio=3:7 ) (50ml×2) to wash the filter cake and ...
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