Houttuynia cordata extract feed additive and preparation method thereof
A technology of Houttuynia cordata extract and feed additive, applied in the field of Houttuynia cordata extract feed additive and its preparation, to achieve the effects of reducing the incidence of PRRS, high content of active components, and high yield of extract
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[0029] Example 1
[0030] This embodiment relates to a feed additive of Houttuynia cordata extract; its preparation specifically includes the following steps:
[0031] Step 1. Dry the houttuynia cordata leaves naturally, remove impurities, dry them at 60°C for 6 hours, pulverize and pass through a sieve with an aperture of 0.6mm, add 12ml of ethanol solution per gram of houttuynia cordata, and add 70wt% ethanol solution for immersion for 4 hours; Add it to an ultrasonic extractor and perform ultrasonic extraction at room temperature and 115KHz for 45 minutes; after extraction, filter to obtain filtrate and solid residue a; evaporate under reduced pressure to remove ethanol from the filtrate to obtain the first extract;
[0032] Step 2: Add 8 times the amount of water to the solid residue a, boil for 5 hours, with a vapor pressure of 0.5 MPa, and filter to obtain a second extract and solid residue b;
[0033] Step 3: Add 6 times the amount of water to the solid residue b, boil for 3 ho...
Example Embodiment
[0043] Example 2
[0044] The purpose of this embodiment is to consider the influence of pH on the dry paste rate and the extraction rate of active components in the water extraction step after ultrasonic extraction. The preparation of this embodiment is the same as that of embodiment 1, the difference is: in step two, acetic acid is added to adjust the water pH to 5.5, 6.0, 6.5, and in step three, saturated sodium hydroxide is added to adjust the water to pH 8.0, 8.5. , 9.0, forming 9 experimental groups; the pH values of steps 2 and 3 corresponding to experimental groups 1-9 in turn are 5.5, 8.0, 5.5, 8.5, 5.5, 9.0, 6.0, 8.0, 6.0, 8.5, 6.0, 9.0, 6.5, 8.0, 6.5, 8.5, 6.5, 9.0.
[0045] Using 100g of Houttuynia herbal material, a comparative test of this example, example 1 and comparative example 1 was carried out; the details are as follows:
[0046] Dry paste rate determination: The first, second, and third extracts obtained in the above 9 experimental groups and Example 1 were...
Example Embodiment
[0052] Example 3
[0053] This embodiment relates to a feed additive of Houttuynia cordata extract; its preparation is the same as in embodiment 1, except that:
[0054] Step 1. Pass through a sieve with an aperture of 0.5mm, add 10ml of ethanol solution to each gram of Houttuynia cordata, add 65wt% ethanol solution and soak for 5h; ultrasonically extract for 35min under 110KHz;
[0055] Step 2. Boiling for 4h, steam pressure 0.4MPa;
[0056] Step 3: Boiling for 5 hours, steam pressure 1.7MPa.
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