A quasi-in-situ ebsd technique to study the formation mechanism of alloy substrate recrystallization and cubic texture
A quasi-in-situ, sample technology, used in instruments, measuring devices, scientific instruments, etc., can solve the problem of difficult repeated testing of samples
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Embodiment 1
[0020] The quasi-in-situ EBSD technique was used to study the formation mechanism of strong cubic texture at high temperature for u-Ni alloy substrate. Firstly, mark the surface of the studied sample by making a hardness test; secondly, fix the studied sample on the figure 1 On the sample table shown, the EBSD test was performed on the selected area; then, the test sample was taken out, and the heat treatment time was continued to be extended at 1000°C, and the EBSD test was performed on the selected area again; the same sample was tested several times according to the experimental analysis needs Repeat the heat treatment and perform multiple EBSD tests on the same area. Select the four pictures in the quasi-in-situ EBSD test result picture, such as image 3 As shown, the method of the present invention is capable of analyzing the formation mechanism of the cubic texture.
Embodiment 2
[0022] The quasi-in-situ EBSD technique was used to study the recrystallization grain growth mechanism of Ni5W alloy substrate. Since the cross-section of the sample is only 80 μm, it is not suitable to mark the surface of the studied sample by hardness testing, so it is mainly positioned through the scale on the sample stage; first, the studied sample is heat-treated at 700 °C for 5 minutes, fixed at figure 2 On the sample stage shown, the EBSD test is performed on the selected area; then, the test sample is taken out, and the heat treatment time is continued to be extended at 700°C, and the EBSD test is performed on the selected area again. Select two pictures in the quasi-in-situ EBSD test result graph, such as Figure 4 As shown, the method of the present invention is capable of analyzing the recrystallization mechanism.
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