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A kind of method of chitosan/tio2 composite finishing wool fabric

A chitosan and fabric technology, which is applied in ultrasonic/sonic fiber treatment, liquid/gas/steam textile material treatment, vibration treatment, etc., can solve the problems of large environmental pollution of finishing liquid, complicated finishing procedures and poor finishing effect. , to achieve the effect of improving the grafting reaction efficiency and feeling good

Active Publication Date: 2015-10-28
ZHEJIANG ZHONGXIN DYEING & FINISHING CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] What the present invention aims to solve are the defects in the existing wool fabric finishing methods such as poor finishing effect, complicated finishing procedures, and large environmental pollution caused by the finishing liquid.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Embodiment Construction

[0010] The present invention will be further described below in conjunction with embodiment.

[0011] A chitosan / TiO 2 A method for compound finishing wool fabrics, said method at least comprising the following steps: a. fabric pretreatment: washing the wool fabrics and placing them in warm water, and treating them with ultrasonic waves with a frequency of 30-40KHz for 30 minutes; b. preparing a composite finishing solution : Dissolve a certain amount of butyl titanate in a certain volume of ethanol, add a certain amount of diethanolamine, stir evenly, add a certain volume of ethanol and water mixture, continue to stir for a period of time, then raise the temperature and return to the state of reflux After stirring for a period of time, nano-TiO with a concentration of 0.4mol / L was formed. 2 Sol, the molar ratio of butyl titanate, diethanolamine, ethanol and water is 1:0.8:20:0.6; 2 In the sol, add 1.0% owf chitosan, 3.5% owf cross-linking agent citric acid and 1.5% owf cata...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention provides a method for finishing wool fabric by compositing chitosan / TiO2, which comprises the following steps: A)pretreating fabric; B)preparing composite finishing liquor, taking butyl titanate and dissolving in ethanol, adding diethanolamine, uniformly stirring and adding mixed liquor mixed by ethanol and water, heating, stirring under a backflow state to form nano TiO2 sol; adding chitosan, citric acid and sodium hypophosphate in the nano TiO2 sol, uniformly stirring to obtain the composite finishing liquor; C)finishing wool fabric, placing wool fabric in the composite finishing liquor, dipping and padding twice, wherein mangle expression is 85% and padding temperature is 50-65%; D)predrying; E)baking; F)washing; and G)drying. According to the finishing method, chitosan and nano TiO2 sol are employed as the composite finishing liquor, the finished wool fabric has good antibiosis, shrinkproof, ultraviolet resistance and anti-insolation performances; the finishing method generates no pollution on human body and environment, and the finished wool fabric has good hand feeling.

Description

technical field [0001] The present invention relates to a kind of finishing method of wool fabric, especially relate to a kind of using chitosan / TiO 2 A method for compound finishing wool fabric. Background technique [0002] With the widespread use of light and thin fabrics in summer, the deodorization, antibacterial, anti-ultraviolet and sun resistance properties of wool fabrics have become the concerns of textile workers. After long-term ultraviolet irradiation on wool fabric, the dye molecules on the fabric will absorb photons and become excited states, which will cause the dye to undergo photochemical reactions and reduce the light fastness of the fabric. Become an important factor affecting product quality and grade. [0003] Nano-TiO 2 With its excellent chemical stability, high efficiency, selectivity, non-dissolvability, safety, low price, and non-polluting advantages, it is recognized as one of the hot spots in the application research of high-tech textiles....

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M11/46D06M15/03D06M13/207D06M11/70D06M10/02D06B13/00D06B3/18D06B15/00D06B3/10D06M101/12
Inventor 曹月华
Owner ZHEJIANG ZHONGXIN DYEING & FINISHING CO LTD
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