A kind of metal surface silane coating corrosion inhibitor
A technology of metal surface and corrosion inhibitor, applied in the field of preparation of corrosion inhibitor, can solve the problems affecting the use effect of industrial devices and the like
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Embodiment 1
[0026] Step 1. Nano-Fluorocarbon CeFCO 3 Surface polymerization:
[0027] In the 500L reactor, add nano-fluorocarbon cerium CeFCO according to the following ratio 3 Disperse in ethanol, add trifluoroethyl acrylate monomer, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzene sulfonate, etc. in the following proportions, raise the temperature, and react at 80°C for 6 hours to obtain Surface polymerized nano-fluorocarbon cerium CeFCO 3 Micro suspension.
[0028]
[0029] Step 2. Add ionic liquid:
[0030] In a 500L reactor, add nano-fluorocarbon cerium CeFCO 3 97Kg of microsuspension liquid, 3Kg of 1-hexyl-2,3-dimethylimidazole tetrafluoroborate ionic liquid, mixed in the reaction kettle for 20 hours, to obtain the product, numbered SX-1.
Embodiment 2
[0032] Step 1. Nano-Fluorocarbon CeFCO 3 Surface polymerization:
[0033] In the 500L reactor, add nano-fluorocarbon cerium CeFCO according to the following ratio 3 Disperse in ethanol, add trifluoroethyl acrylate monomer, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzene sulfonate, etc. in the following proportions, raise the temperature, and react at 70°C for 10 hours to obtain the Surface polymerized nano-fluorocarbon cerium CeFCO 3 Micro suspension.
[0034]
[0035] Step 2. Add ionic liquid:
[0036] In a 500L reactor, add nano-fluorocarbon cerium CeFCO 3 Micro-suspension 95Kg, 1-hexyl-2,3-dimethylimidazole tetrafluoroborate ionic liquid 5Kg, mixed in the reaction kettle for 40hr to obtain the product, numbered SX-2.
Embodiment 3
[0038] Step 1. Nano-Fluorocarbon CeFCO 3 Surface polymerization:
[0039] In the 500L reactor, add nano-fluorocarbon cerium CeFCO according to the following ratio 3 Disperse into ethanol, add trifluoroethyl acrylate monomer, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzene sulfonate, etc. in the following proportions, increase the temperature, and react at 60°C for 15 hours to obtain the Surface polymerized nano-fluorocarbon cerium CeFCO 3 Micro suspension.
[0040]
[0041] Step 2. Add ionic liquid:
[0042] In a 500L reactor, add nano-fluorocarbon cerium CeFCO 3 Micro-suspension 99Kg, 1-hexyl-2,3-dimethylimidazole tetrafluoroborate ionic liquid 1Kg, mixed in the reaction kettle for 10hr to obtain the product, numbered SX-3.
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