The invention discloses sulfonated
polyether ether ketone and a preparation method thereof, and relates to the technical field of
high polymer materials, the method comprises the following steps: taking 4, 4 '-difluorobenzophenone,
bisphenol A and
potassium 2, 5-dihydroxybenzenesulfonate as raw materials, taking
potassium carbonate as a catalyst, taking
dimethyl sulfoxide and
xylene as solvents, stirring and introducing
nitrogen, and reacting at 140 DEG C for 90 minutes; raising the temperature to 155 DEG C, continuously reacting, and separating
condensed water and
xylene out of a
reaction system in the reaction process; adding an end-capping
reagent to terminate the reaction to obtain a yellow jelly; introducing the yellow jelly into
ethanol, soaking, crushing, washing and
drying to obtain sulfonated polyether-
ether-
ketone; in the first step, the particle size of the
potassium carbonate is 30-300 meshes. By adopting
potassium carbonate with smaller particle size, the temperature of the
condensation reaction can be reduced from 180 DEG C to 155 DEG C, and the reaction time is shortened, so that the
decomposition of
dimethyl sulfoxide can be avoided, no malodorous gas is generated in the preparation process, the potential safety
hazard is eliminated, and the purity of the product is improved.