Recovery and regeneration method of clogged deactivated scr catalyst and regenerated scr catalyst carrier
A SCR catalyst and catalyst technology, applied in the field of regenerated SCR catalyst carrier, can solve the problems of low actual use value, high cost, and low catalyst activity recovery ability, and achieve good catalytic activity, mechanical strength, and high activity recovery ability.
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Embodiment 1
[0033]Weigh 25 kg of waste catalyst (blocked and deactivated catalyst), crush it into small pieces of 0.5-1cm by a plastic crusher, pass through a 50-mesh vibrating sieve, and add water to wash the dust, and put the washed catalyst fragments into 60 kg concentration Soak in 1M dilute nitric acid for 1-2 hours, filter, wet pulverize with a pulverizer, add 50 kg of water, control the concentration of the catalyst slurry at 26wt%, put it into a sand mill for ultrafine pulverization, and take a sample to detect that the particle diameter is 20-45nm Qualified; unqualified secondary beating;
[0034] Put the qualified catalyst slurry into the slurry tank, add pure water until titanium dioxide accounts for about 23wt% of the slurry, add ammonia water to adjust the pH to 7.5, add ammonium paratungstate and white carbon black, and the addition amount meets the following requirements: WO 3 The content accounts for 5wt% of the regeneration carrier, SiO 2 The content accounts for 5wt% of...
Embodiment 2
[0037] Weigh 25 kg of waste catalyst, break it into small pieces of 0.5-1cm by a plastic crusher, pass through a 50-mesh vibrating sieve, add water to wash the dust, put the washed catalyst fragments into 60 kg of dilute nitric acid with a concentration of 1M and soak 1-2 hours, after filtration, wet pulverization by pulverizer, add water to adjust the concentration of catalyst slurry to control at 30wt%, put it into sand mill for superfine pulverization, and take samples to detect that the particle diameter is 45-100nm is qualified; unqualified secondary beating ;
[0038] Put the qualified catalyst slurry into the slurry tank, add pure water until titanium dioxide accounts for about 23wt% of the slurry, add ammonia water to adjust the pH to 8.0, add ammonium paratungstate and white carbon black, and the addition amount meets the following requirements: WO 3 The content accounts for 5wt% of the regeneration carrier, SiO 2 The content accounts for 5wt% of the regenerated carr...
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