Reactor for preparing iron oxide red

An iron oxide red, reactor technology, applied in iron oxide, iron oxide/iron hydroxide, chemical/physical/physical-chemical stationary reactors, etc., can solve the problem of uneven distribution of product particles, dead corners of reaction, and decreased reaction efficiency And other issues

Inactive Publication Date: 2015-05-13
ZHENJIANG JINSHENGYUAN INFORMATION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this case, the distribution of the gas-liquid-solid flow field in the gas-liquid-solid three-phase reactor is extremely important. If the design is unreasonable, it will cause a dead angle in the reaction, resulting in a decrease in the effective reaction volume of the reactor, a decrease in reaction efficiency, and uneven distribution of product particles. The quality has declined, and there are few designs for preparing iron oxide red reactors in the current public reports. For example, the invention patent "Wet Process and Equipment for Manufacturing Iron Oxide Red" (CN1143049A) discloses a production process for iron oxide red, but Simpler requirements for reaction equipment

Method used

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  • Reactor for preparing iron oxide red

Examples

Experimental program
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Effect test

Embodiment 1

[0012] Below in conjunction with accompanying drawing, the present invention will be further described: the schematic diagram of the reactor mechanism of preparing iron oxide red provided by the present invention is as follows figure 1 Shown: by the reaction tank, frequency conversion motor. Main shaft, conical distribution plate, fixing device, first stirring impeller, second stirring impeller, heating coil, aeration pan, sewage outlet and thermometer; among them, a frequency conversion motor is installed in the center of the top of the reaction tank, and the frequency conversion motor is connected to the main shaft, the main shaft The first stirring paddle and the second stirring paddle are respectively installed up and down. The conical air distribution plate is fixed on the inner wall of the reaction tank through a fixing device and its height is between the first stirring paddle and the second stirring paddle. The bottom of the reaction tank is equipped with Aeration pan,...

Embodiment 2

[0014] The device in this embodiment is the same as in Embodiment 1, wherein the conical distribution plate is a porous plastic plate with a circular through hole on the surface, and the empty area is 1 cm 2 , the number of empty spaces per square meter is 5000.

[0015] Add the reaction raw material ferrous sulfate solution into the reaction tank, add sodium hydroxide solution to adjust the pH value to 8, feed steam to the heating coil to 75 degrees, feed air from the aeration plate at the bottom of the reaction tank, and start the frequency conversion motor to drive the stirring The paddle rotates and stirs, and the air entering from the aeration plate at the bottom of the reaction tank enters the upper part of the reaction tank through the conical air distribution plate, and the reaction materials in the reaction tank are fully mixed. After 2.5 hours of reaction, the color paste in the reaction tank meets the requirements, and the reaction is stopped. Compared with conventi...

Embodiment 3

[0017] The structure of the reactor in this example is the same as in Example 1, wherein the conical air distribution plate is a porous stainless steel plate with square through holes on the surface; the hole diameter is 10 cm, and the number of holes per square meter is 80.

[0018] Add the reaction raw material ferrous sulfate solution into the reaction tank, add sodium hydroxide solution to adjust the pH value to 9, feed steam to the heating coil to 90 degrees, feed air from the aeration tray at the bottom of the reaction tank, and start the frequency conversion motor to drive the stirring The paddle rotates and stirs, and the air entering from the aeration plate at the bottom of the reaction tank enters the upper part of the reaction tank through the conical air distribution plate, and the reaction materials in the reaction tank are fully mixed. After 2 hours of reaction, the color paste in the reaction tank meets the requirements, and the reaction is stopped. Compared with...

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Abstract

The present invention relates to a reactor for preparing iron oxide red. The reactor comprises a reaction tank, a variable-frequency motor, a main shaft, stirring paddles, a heating coil pipe, aeration disks and a conical air distribution plate, wherein the top portion of the reaction tank is provided with the variable-frequency motor and the main shaft, the main shaft is provided with two sets of the stirring paddles, the conical air distribution plate is arranged between the two sets of the stirring paddles and on the inner wall of the reaction tank, and the bottom portion of the reaction tank is provided with the heating coil pipe and the aeration disks. According to the present invention, the frequency converter is utilized to control the variable-frequency motor so as to achieve different stirring rates and control the mixing uniformity of the liquid in the reaction tank; and the air required by the reaction is introduced into the aeration disks on the bottom portion, and rises to the conical air distribution plate so as to be secondarily and uniformly dispersed.

Description

technical field [0001] The invention relates to a reactor for preparing iron oxide red in an inorganic pigment iron oxide red production system, in particular to a gas-liquid-solid three-phase reactor for preparing iron oxide red. Background technique [0002] Iron oxide is an important inorganic chemical pigment, and iron oxide red is a relatively common one, which is widely used in coatings, construction, transportation and other fields. At present, the production methods of iron oxide pigments include dry method and wet method. A large amount of waste gas is produced in the dry production process, the environmental pollution is serious, and it is not practical in a large amount; the wet method is a method commonly used in industry at present. In the production process of wet production of iron oxide, cylindrical reaction tanks are generally used for reaction . The reaction raw material ferrous sulfate solution is added to the reaction tank, and sodium hydroxide solution...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/18C01G49/06
CPCB01J19/0006B01J19/18B01J2219/00049B01J2219/00184B01J2219/185C01G49/06Y02P20/10
Inventor 盛淑芳
Owner ZHENJIANG JINSHENGYUAN INFORMATION TECH
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