Method for producing hydrogenated diesel oil with low freezing point
A production method and diesel oil technology, which is applied in the fields of hydrotreating process, petroleum industry, and hydrocarbon oil treatment, etc., can solve the problems of high reaction temperature at the outlet of the bed layer, limitation of operation cycle, etc., and achieve the improvement of yield and cetane number, The effect of reducing hot spot temperature and saving operating costs
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Embodiment 1
[0042] use figure 1 The process flow shown is to produce low-condensation-point diesel by means of mixing and grading series processes. In embodiment 1, two hydrogenation reaction zones connected in series are included, and in the composite bed of the depreciating and upgrading catalyst in each reaction zone, the mixing volume ratio of the hydrogenation depreciating catalyst and the hydrogenation and upgrading catalyst is 1:2, and the catalyst The total amount is the same as that of Comparative Example 1 and Comparative Example 2. The hydrogenation upgrading catalyst used in Example 1 is FC-18 catalyst, and the hydrodecondensation catalyst is FDW-3 catalyst, both of which are commercial catalysts developed and produced by Fushun Petrochemical Research Institute.
[0043] The operating conditions and test results are listed in Table 3.
Embodiment 2
[0045] use figure 1 The process flow shown is to produce low-condensation-point diesel oil by using gradation series and mixed packing process. In Example 1, two hydrogenation reaction zones connected in series are included. In the composite bed of the combined depreciation catalyst in each reaction zone, the mixing volume ratio of the hydrogenation depreciation catalyst and the hydrogenation upgrading catalyst is 1:2, and the total amount of catalyst is 1:2. Consumption is all the same as Comparative Example 1 and Comparative Example 2. The hydromodified isomerization depreciation catalyst used in Example 2 is FC-18G catalyst, and the hydrodegradation catalyst is FDW-3 catalyst, both of which are commercial catalysts developed and produced by Fushun Petrochemical Research Institute.
[0046] Table 2 Raw oil properties table.
[0047] project Raw oil source Often three-line diesel Density(20℃) / g·cm -3 0.8808 Distillation range / ℃ 270~390 Ni...
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