A kind of flue-cured tobacco extract and electronic cigarette liquid
A technology of extract and flue-cured tobacco, which is applied in the field of flue-cured tobacco extract and e-liquid, can solve the problems of e-liquid lack of tobacco aroma characteristics, weak tobacco aroma characteristics, and miscellaneous gas in extraction products, so as to avoid excessive chemical reactions and improve extraction efficiency The effect of increasing and extracting less impurities
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Embodiment 1
[0032] Soak 110g of Zimbabwean L10F shredded tobacco in 200mL of absolute ethanol for 4h, and extract it with the improved Soxhlet extraction device of the present invention for 3h, the vacuum degree is 40mmHg, the heating temperature of the water bath is 50°C, the extract is concentrated under reduced pressure until the solvent is dry, and the concentrate is obtained by (5mL water + 5mL absolute ethanol + 20mL glycerin) was dissolved, flavored as e-cigarette liquid, and prepared as a test sample. The e-cigarette produced in the comparative example was used as a control, and the sensory evaluation was carried out. The result of the evaluation and evaluation was: it has obvious characteristics of Zimbabwean smoke, and the smoke is fuller and more mellow. Compared with the control, the flue gas of the test sample is purer. The GC-MS picture of the flue-cured tobacco extract obtained figure 2 As shown, because the peak of nicotine is too large, in order to clearly show other co...
Embodiment 2
[0034] Soak 10g of Zimbabwe L10F with 200mL of n-hexane for 4h, extract with the improved Soxhlet extraction device of the present invention for 3h, the vacuum degree is 80mmHg, the water bath heating temperature is 45°C, the extract is concentrated under reduced pressure until the solvent is dry, and the concentrate is extracted with (5mL Water + 5mL absolute ethanol + 20mL glycerin) dissolved, flavored as e-cigarette liquid, and tested. Taking the e-liquid prepared in Example 1 as a control, the sensory evaluation and smoking evaluation results are as follows: Compared with the control, the test sample has more energy, a stronger sense of satisfaction, and a little miscellaneous gas.
[0035] image 3 It is the GC-MS figure and figure 2 superposition. From image 3 It can be seen that ethanol is a polar solvent, while n-hexane is used as a non-polar solvent, and the aroma components extracted by the non-polar solvent n-hexane are densely distributed in the area with a sh...
Embodiment 3
[0037] Soak Sangzhi B3F Zimbabwe L10F in 200mL of n-hexane for 4h, extract for 3h with the improved Soxhlet extraction device of the present invention, vacuum degree is 80mmHg, water bath heating temperature is 45°C, the extract is concentrated under reduced pressure until the solvent is dry, and the concentrate is (5mL water + 5mL absolute ethanol + 20mL glycerin) is dissolved and used as the e-cigarette liquid for flavoring. Make two samples, one with 0.5ml of commercially available e-cigarette liquid as a control sample; the other as an experimental sample, add 0.5ml of the same commercially available e-cigarette liquid as the control sample, and add another 0.25ml prepared in this example The smoke liquid was extracted from the flue-cured tobacco, and the results of the comparative evaluation and smoking evaluation are as follows: Compared with the control sample, the experimental sample has obvious characteristics of tobacco aroma, strong vigor and strong sense of satisfac...
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