A kind of modified hydroxyethyl cellulose tackifier for drilling and preparation method thereof
A technology of hydroxyethyl cellulose and thickening agent, which is applied in the field of polymers, can solve the problems of loss of thickening effect and poor salt resistance, and achieve the effect of simple preparation method, thickening effect and strong salt resistance
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[0030] In a 500ml three-neck flask, 30g of hydroxyethylcellulose and 10g of sodium p-styrenesulfonate were fully dissolved in 300ml of deionized water to obtain a reaction solution. Accurately weigh 0.2 g of ammonium persulfate, fully dissolve it with 20 ml of deionized water and transfer the solution to a constant pressure separatory funnel. Nitrogen was blown into the reaction flask to remove air, and the temperature of the system was raised to 50°C. The ammonium persulfate solution was added dropwise through a constant pressure separatory funnel for reaction. After 8 hours, the reacted mixed solution was immersed in sufficient acetone for precipitation to obtain a polymer. Dry and grind into powder to obtain the graft copolymer of hydroxyethyl cellulose / sodium p-styrene sulfonate.
[0031] 2. Infrared Spectrum Test and Analysis of Modified Hydroxyethyl Cellulose Viscosifier for Well Drilling
[0032] figure 1 It is the Fourier transform infrared spectrum test of the tack...
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