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A quality detection method of pepper powder based on component analysis

A quality detection method and component analysis technology, applied in the direction of analyzing materials, measuring devices, material separation, etc., to achieve high accuracy, good method reproducibility, and stable and reliable results

Inactive Publication Date: 2017-03-22
ZENGCHENG HANDYWARE SEASONING
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] In view of the lack of a complete and effective quality detection technology for pepper powder, it is necessary to develop a simple, rapid, stable and reliable quality detection method for pepper powder to fill the gap in the existing technology

Method used

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  • A quality detection method of pepper powder based on component analysis
  • A quality detection method of pepper powder based on component analysis
  • A quality detection method of pepper powder based on component analysis

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Experimental program
Comparison scheme
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Embodiment 1

[0034] Embodiment 1, the Chinese prickly ash powder quality detection method based on component analysis

[0035] 1. Experimental reagents and instruments:

[0036] 1.1 Reagents: ethanol (analytical grade), phenylethyl propionate, linalool, linalyl acetate, β-caryophyllene, α-caryophyllene, purified water.

[0037] 1.2 Instruments: GC7890A-5973C gas chromatography mass spectrometer (Aglient, USA), electronic balance, reflux device.

[0038] ,experimental method:

[0039] 2.1 Experimental conditions:

[0040] 2.1.1 Chromatographic conditions of gas chromatography mass spectrometer: non-polar chromatographic column: HP-5MS (30 m x 250 μm x0.25 μm); carrier gas: high-purity helium; column flow rate: 1mL / min constant flow; split ratio : 1:1, inlet temperature: 250°C; injection volume: 1μL; temperature program: column initial temperature 60°C, keep for 2min, rise to 150°C at a rate of 3°C / min, keep for 1min, then increase to 15°C Ramp to 280°C at a rate of 1 / min and hold for 4 mi...

Embodiment 2

[0048] Embodiment 2, the Chinese prickly ash powder quality detection method based on component analysis

[0049] The present embodiment takes the Zanthoxylum bungeanum sample that numbering is HD11008 as detection object, carries out the test to the Zanthoxylum bungeanum sample of 10 batches with the operation method of the embodiment of the present invention 1, each sample is measured in parallel twice, respectively to the aroma in Zanthoxylum bungeanum powder. camphor, linalyl acetate, β-caryophyllene and meth-caryophyllene were quantified, and the content range was ±10% of the test result (average value). The results are shown in Table 1 below.

[0050] Table 1 Contents of linalool, linalyl acetate, caryophyllene and caryophyllene in Zanthoxylum bungeanum powder

[0051]

[0052] It can be seen from the above table 1 that through the controllable sample pretreatment steps, the obtained Zanthoxylum bungeanum extract was quantitatively analyzed by gas chromatography-mass ...

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Abstract

The invention discloses a method for detecting the quality of pepper powder based on component analysis. A certain amount of the pepper powder is distilled through water vapor to prepare a pepper extract solution, the obtained pepper extract solution is subjected to component analysis through a gas chromatographic mass spectrometry method, characteristic chemical components including linalool, linalyl acetate, beta-caryophyllene and alpha-caryophyllene in the pepper extract solution are selected as main target components, phenylethyl propionate is selected as an internal standard substance, and linalool, linalyl acetate, beta-caryophyllene and alpha-caryophyllene in the pepper extract solution are quantitatively analyzed with a selected ion gas chromatographic mass spectrometry method to determine the content and range of linalool, linalyl acetate, beta-caryophyllene and alpha-caryophyllene. The method for detecting the quality of the pepper powder based on the component analysis is capable of quickly, simply, flexibly and accurately detecting the quality of the pepper powder and can be widely applied.

Description

technical field [0001] The invention belongs to the technical field of condiment quality detection, and relates to a method for detecting the quality of pepper powder based on component analysis, specifically referring to the detection of linalool, linalyl acetate, and acetylene in pepper powder by gas chromatography-mass spectrometry. Method for quality determination of caryophyllene and caryophyllene content. Background technique [0002] In recent years, in the field of food safety in my country, various incidents of adulterated and counterfeit food have occurred frequently. People's material living standards are improving day by day, but the color and fragrance of the delicacies on the table are greatly reduced, the prickly ash is not numb, the chili is not spicy, and the sesame oil is not fragrant. Adulteration of seasoning powder as a raw material for food production is not uncommon. The general method of counterfeiting is to mix other substances with lower prices in ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02
Inventor 梁俪恩王延平李永南
Owner ZENGCHENG HANDYWARE SEASONING
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