Rubber composition for tires, and pneumatic tire using same
A rubber composition and tire technology, applied in the field of pneumatic tires and rubber compositions for tires, can solve the problems of insufficient reduction in rolling resistance wet road performance, high agglomeration, low affinity between silica and rubber components, etc. problems, to achieve the effects of excellent wet performance, excellent processability, and excellent wear resistance
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[0180] Hereinafter, examples are shown to specifically explain the present invention. However, the present invention is not limited to this.
[0181]
[0182] In a 2L separable flask equipped with a stirrer, a reflux cooler, a dropping funnel and a thermometer, 107.8g of bis(triethoxysilylpropyl)tetrasulfide (KBE-846 manufactured by Shin-Etsu Chemical Industry) (0.2mol), γ-mercaptopropyltriethoxysilane (KBE-803 manufactured by Shin-Etsu Chemical Industry) 190.8g (0.8mol), Octyltriethoxysilane (KBE-3083 manufactured by Shin-Etsu Chemical Industry) 442.4g ( 1.6 mol), 190.0 g of ethanol, and then a mixed solution of 37.8 g (2.1 mol) of 0.5N hydrochloric acid and 75.6 g of ethanol was added dropwise at room temperature. Then, it was stirred at 80°C for 2 hours. Then, it filtered, 17.0g of 5% KOH / EtOH solution was dripped, and it stirred at 80 degreeC for 2 hours. Then, it was concentrated under reduced pressure and filtered to obtain 480.1 g of polysiloxane as a brown transparent ...
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